5'-(S)-C-(azidomethyl)-3'-O-(tert-butyldimethylsilyl)-5'-O-pixylthymidine

Base Information

Chemical Name:5'-(S)-C-(azidomethyl)-3'-O-(tert-butyldimethylsilyl)-5'-O-pixylthymidine
CAS No.:1260530-50-4
Molecular Formula:C₃₆H₄₁N₅O₆Si
Molecular Weight:667.837
Hs Code.:

Synonyms:5'-(S)-C-(azidomethyl)-3'-O-(tert-butyldimethylsilyl)-5'-O-pixylthymidine

Suppliers and Price of 5'-(S)-C-(azidomethyl)-3'-O-(tert-butyldimethylsilyl)-5'-O-pixylthymidine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5'-(S)-C-(azidomethyl)-3'-O-(tert-butyldimethylsilyl)-5'-O-pixylthymidine

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Technology Process of 5'-(S)-C-(azidomethyl)-3'-O-(tert-butyldimethylsilyl)-5'-O-pixylthymidine

There total 1 articles about 5'-(S)-C-(azidomethyl)-3'-O-(tert-butyldimethylsilyl)-5'-O-pixylthymidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 42506-03-6
pixyl chloride

: 177490-90-3
5'-(S)-C-(azidomethyl)-3'-O-(tert-butyldimethylsilyl)thymidine

: 1260530-50-4
5'-(S)-C-(azidomethyl)-3'-O-(tert-butyldimethylsilyl)-5'-O-pixylthymidine

Guidance literature:: With dmap; In N,N-dimethyl-formamide; at 120 ℃; for 0.5h; Inert atmosphere; Microwave irradiation;
DOI:10.1002/chem.201001253

Reference yield: 92.0%

: 1260530-50-4
5'-(S)-C-(azidomethyl)-3'-O-(tert-butyldimethylsilyl)-5'-O-pixylthymidine

: 536-74-3
phenylacetylene

: 1260530-51-5
3'-O-(tert-butyldimethylsilyl)-5'-(S)-C-(4-phenyl-1,2,3-triazol-1-yl)methyl-5'-O-pixylthymidine

Guidance literature:: With pyridine; copper(ll) sulfate pentahydrate; sodium L-ascorbate; In tetrahydrofuran; water; at 20 ℃; for 3h;
DOI:10.1002/chem.201001253

Reference yield: 88.0%

: 1260530-50-4
5'-(S)-C-(azidomethyl)-3'-O-(tert-butyldimethylsilyl)-5'-O-pixylthymidine

: 1066-54-2
trimethylsilylacetylene

: 1260530-57-1
3'-O-(tert-butyldimethylsilyl)-5'-O-pixyl-5'-(S)-C-(4-(trimethylsilyl)-1,2,3-triazol-1-yl)methylthymidine

Guidance literature:: With pyridine; copper(ll) sulfate pentahydrate; sodium L-ascorbate; In water; tert-butyl alcohol; at 20 ℃; for 19h;
DOI:10.1002/chem.201001253