2-(1-benzyl-1-phenyl-propyl)-3,4-dimethyl-5-phenyl-4,5-dihydro-oxazol-3-ium; trifluoro-methanesulfonate

Base Information

Chemical Name:2-(1-benzyl-1-phenyl-propyl)-3,4-dimethyl-5-phenyl-4,5-dihydro-oxazol-3-ium; trifluoro-methanesulfonate
CAS No.:925675-38-3
Molecular Formula:CF₃O₃S*C₂₇H₃₀NO
Molecular Weight:533.612
Hs Code.:

Synonyms:2-(1-benzyl-1-phenyl-propyl)-3,4-dimethyl-5-phenyl-4,5-dihydro-oxazol-3-ium; trifluoro-methanesulfonate

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Chemical Property of 2-(1-benzyl-1-phenyl-propyl)-3,4-dimethyl-5-phenyl-4,5-dihydro-oxazol-3-ium; trifluoro-methanesulfonate

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Technology Process of 2-(1-benzyl-1-phenyl-propyl)-3,4-dimethyl-5-phenyl-4,5-dihydro-oxazol-3-ium; trifluoro-methanesulfonate

There total 2 articles about 2-(1-benzyl-1-phenyl-propyl)-3,4-dimethyl-5-phenyl-4,5-dihydro-oxazol-3-ium; trifluoro-methanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 358-23-6
trifluoromethylsulfonic anhydride

: 1068601-51-3
(R)-2-benzyl-N-[(1S,2S)-2-hydroxy-1-methyl-2-phenylethyl]-N-methyl-2-phenylbutanamide

: 925675-38-3
2-(1-benzyl-1-phenyl-propyl)-3,4-dimethyl-5-phenyl-4,5-dihydro-oxazol-3-ium; trifluoro-methanesulfonate

Guidance literature:: With pyridine; In dichloromethane; at 0 ℃; for 0.166667h; optical yield given as %de; Inert atmosphere;
DOI:10.1021/ja806021y

Reference yield:

: 2-benzyl-N-(2-hydroxy-1-methyl-2-phenyl-ethyl)-N-methyl-2-phenyl-butyramide

: 358-23-6
trifluoromethylsulfonic anhydride

: 925675-38-3
2-(1-benzyl-1-phenyl-propyl)-3,4-dimethyl-5-phenyl-4,5-dihydro-oxazol-3-ium; trifluoro-methanesulfonate

: 2-(1-benzyl-1-phenyl-propyl)-3,4-dimethyl-5-phenyl-4,5-dihydro-oxazol-3-ium; trifluoro-methanesulfonate

Guidance literature:: With pyridine; In dichloromethane; at 0 ℃; for 0.0333333h; Title compound not separated from byproducts;
DOI:10.1021/ol0628762

Reference yield:

: 925675-38-3
2-(1-benzyl-1-phenyl-propyl)-3,4-dimethyl-5-phenyl-4,5-dihydro-oxazol-3-ium; trifluoro-methanesulfonate

: 1068602-72-1
(2R)-2-benzyl-2-phenylbutanal

Guidance literature:: 2-(1-benzyl-1-phenyl-propyl)-3,4-dimethyl-5-phenyl-4,5-dihydro-oxazol-3-ium; trifluoro-methanesulfonate; With sodium bis(2-methoxyethoxy)aluminium dihydride; In tetrahydrofuran; toluene; at 0 ℃; for 0.333333h; Inert atmosphere;

With hydrogenchloride; trifluoroacetic acid; In tetrahydrofuran; water; toluene; at 0 - 50 ℃; Inert atmosphere;
DOI:10.1021/ja806021y