1,1,1-trichloro-3-[2-(2-methyl-propane-1-sulfonyl)-4,6-dinitro-phenyl]-propan-2-ol

Base Information

Chemical Name:1,1,1-trichloro-3-[2-(2-methyl-propane-1-sulfonyl)-4,6-dinitro-phenyl]-propan-2-ol
CAS No.:472999-08-9
Molecular Formula:C₁₃H₁₅Cl₃N₂O₇S
Molecular Weight:449.696
Hs Code.:

Synonyms:1,1,1-trichloro-3-[2-(2-methyl-propane-1-sulfonyl)-4,6-dinitro-phenyl]-propan-2-ol

Suppliers and Price of 1,1,1-trichloro-3-[2-(2-methyl-propane-1-sulfonyl)-4,6-dinitro-phenyl]-propan-2-ol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of 1,1,1-trichloro-3-[2-(2-methyl-propane-1-sulfonyl)-4,6-dinitro-phenyl]-propan-2-ol

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Hazard Codes:

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Technology Process of 1,1,1-trichloro-3-[2-(2-methyl-propane-1-sulfonyl)-4,6-dinitro-phenyl]-propan-2-ol

There total 3 articles about 1,1,1-trichloro-3-[2-(2-methyl-propane-1-sulfonyl)-4,6-dinitro-phenyl]-propan-2-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 75-87-6
chloral

: 367925-10-8
2-methyl-1-(2-methyl-propane-1-sulfonyl)-3,5-dinitro-benzene

: 472999-08-9
1,1,1-trichloro-3-[2-(2-methyl-propane-1-sulfonyl)-4,6-dinitro-phenyl]-propan-2-ol

Guidance literature:: With potassium carbonate; In tetrahydrofuran; for 1h; Heating;
DOI:10.1081/SCC-120003645

Reference yield:

: 118-96-7
2,4,6-Trinitrotoluene

: 472999-08-9
1,1,1-trichloro-3-[2-(2-methyl-propane-1-sulfonyl)-4,6-dinitro-phenyl]-propan-2-ol

Guidance literature:: Multi-step reaction with 3 steps

1: K₂CO₃; NMP

2: H₂O₂; acetic acid / Heating

3: 75 percent / K₂CO₃ / tetrahydrofuran / 1 h / Heating

With 1-methyl-pyrrolidin-2-one; dihydrogen peroxide; potassium carbonate; acetic acid; In tetrahydrofuran;
DOI:10.1081/SCC-120003645

Reference yield:

: 367924-99-0
1-isobutylsulfanyl-2-methyl-3,5-dinitro-benzene

: 472999-08-9
1,1,1-trichloro-3-[2-(2-methyl-propane-1-sulfonyl)-4,6-dinitro-phenyl]-propan-2-ol

Guidance literature:: Multi-step reaction with 2 steps

1: H₂O₂; acetic acid / Heating

2: 75 percent / K₂CO₃ / tetrahydrofuran / 1 h / Heating

With dihydrogen peroxide; potassium carbonate; acetic acid; In tetrahydrofuran;
DOI:10.1081/SCC-120003645