trans-2,3,4,6-tetra-O-benzyl-1-deoxy-1-(prop-1'-enyl)-α-D-galactopyranose

Base Information

Chemical Name:trans-2,3,4,6-tetra-O-benzyl-1-deoxy-1-(prop-1'-enyl)-α-D-galactopyranose
CAS No.:799267-93-9
Molecular Formula:C₃₇H₄₀O₅
Molecular Weight:564.722
Hs Code.:

Synonyms:trans-2,3,4,6-tetra-O-benzyl-1-deoxy-1-(prop-1'-enyl)-α-D-galactopyranose

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Chemical Property of trans-2,3,4,6-tetra-O-benzyl-1-deoxy-1-(prop-1'-enyl)-α-D-galactopyranose

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Technology Process of trans-2,3,4,6-tetra-O-benzyl-1-deoxy-1-(prop-1'-enyl)-α-D-galactopyranose

There total 6 articles about trans-2,3,4,6-tetra-O-benzyl-1-deoxy-1-(prop-1'-enyl)-α-D-galactopyranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 82659-55-0
3-(2',3',4',6'-tetra-O-benzyl-α-D-galactopyranosyl)prop-1-ene

: 799267-93-9
trans-2,3,4,6-tetra-O-benzyl-1-deoxy-1-(prop-1'-enyl)-α-D-galactopyranose

Guidance literature:: cyclooctadiene-bis(methyldiphenylphosphine)-iridium hexafluorophosphate; In tetrahydrofuran; at 20 ℃; for 48h;
DOI:10.1021/ol060671n

Reference yield:

: 82659-55-0
3-(2',3',4',6'-tetra-O-benzyl-α-D-galactopyranosyl)prop-1-ene

: C₃₇H₄₀O₅

: 799267-93-9
trans-2,3,4,6-tetra-O-benzyl-1-deoxy-1-(prop-1'-enyl)-α-D-galactopyranose

Guidance literature:: With bis(benzonitrile)palladium(II) dichloride; In benzene; for 20h; Heating / reflux;

Reference yield:

: 25878-60-8
D-galactose pentaacetate

: C₃₇H₄₀O₅

: 799267-93-9
trans-2,3,4,6-tetra-O-benzyl-1-deoxy-1-(prop-1'-enyl)-α-D-galactopyranose

Guidance literature:: Multi-step reaction with 4 steps

1: boron trifluoride diethyl etherate / 72 h / 0 - 10 °C

2: methanol; sodium methylate / 1 h / 20 °C

3: tetra-(n-butyl)ammonium iodide; sodium hydride / N,N-dimethyl-formamide / 14 h / 20 °C

4: bis(benzonitrile)palladium(II) dichloride / benzene / 20 h / Heating / reflux

With methanol; bis(benzonitrile)palladium(II) dichloride; boron trifluoride diethyl etherate; sodium methylate; tetra-(n-butyl)ammonium iodide; sodium hydride; In N,N-dimethyl-formamide; benzene;