2,3,4,6-tetra-O-benzyl-1-deoxy-α-D-galactopyranosylethene

Base Information

Chemical Name:2,3,4,6-tetra-O-benzyl-1-deoxy-α-D-galactopyranosylethene
CAS No.:799267-94-0
Molecular Formula:C₃₆H₃₈O₅
Molecular Weight:550.695
Hs Code.:

Synonyms:2,3,4,6-tetra-O-benzyl-1-deoxy-α-D-galactopyranosylethene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2,3,4,6-tetra-O-benzyl-1-deoxy-α-D-galactopyranosylethene

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Technology Process of 2,3,4,6-tetra-O-benzyl-1-deoxy-α-D-galactopyranosylethene

There total 13 articles about 2,3,4,6-tetra-O-benzyl-1-deoxy-α-D-galactopyranosylethene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 287962-77-0
(2R,3S,4R,5S,6R)-3,4,5-tribenzyloxy-2-(benzyloxymethyl)-6-ethynyl-tetrahydropyran

: 799267-94-0
2,3,4,6-tetra-O-benzyl-1-deoxy-α-D-galactopyranosylethene

Guidance literature:: With hydrogen; Lindlar's catalyst; In ethyl acetate; at 20 ℃; for 1h;
DOI:10.1021/ol0482137

Reference yield: 91.0%

: 74-85-1
ethene

: 799267-93-9
trans-2,3,4,6-tetra-O-benzyl-1-deoxy-1-(prop-1'-enyl)-α-D-galactopyranose

: 799267-94-0
2,3,4,6-tetra-O-benzyl-1-deoxy-α-D-galactopyranosylethene

Guidance literature:: With tricyclohexylphosphine; PhCH=Ru[1,3-bis(2,4,6-Me₃C₆H₂)-2-imidazolidinylidene]Cl₂; In dichloromethane; Heating;
DOI:10.1021/ol0482137

Reference yield: 80.0%

: 865880-61-1
C₃₇H₄₀O₅

: 799267-94-0
2,3,4,6-tetra-O-benzyl-1-deoxy-α-D-galactopyranosylethene

Guidance literature:: With ethene; tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; for 72h;

upstream raw materials:

ethene

trans-2,3,4,6-tetra-O-benzyl-1-deoxy-1-(prop-1'-enyl)-α-D-galactopyranose

(2R,3S,4R,5S,6R)-3,4,5-tribenzyloxy-2-(benzyloxymethyl)-6-ethynyl-tetrahydropyran

2,3,4,6-tetra-O-benzyl-α-D-galactopyranosyl iodide

Downstream raw materials:

4-C-(2,3,4,6-tetra-O-benzyl-α-D-galactopyranosyl)-3-E-butene-1,2(S)-di-O-acetate

4-C-(2,3,4,6-tetra-O-benzyl-α-D-galactopyranosyl)-1-O-palmitoyl-2(S)-O-stearoyl-3-E-butene

4-C-(2,3,4,6-tetra-O-benzyl-α-D-galactopyranosyl)-1-O-palmitoyl-3-E-buten-2(S)-ol

[(E)-(S)-1-((4S,5R)-2,2-Dimethyl-5-tetradecyl-[1,3]dioxolan-4-yl)-3-((2R,3S,4R,5S,6R)-3,4,5-tris-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-2-yl)-allyl]-carbamic acid tert-butyl ester

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