1-(2,4-dimethoxyphenyl)-1-(6-methylpyridin-2-yl)methanamine hydrochloride

Base Information

Chemical Name:1-(2,4-dimethoxyphenyl)-1-(6-methylpyridin-2-yl)methanamine hydrochloride
CAS No.:1187993-14-1
Molecular Formula:C₁₅H₁₈N₂O₂*ClH
Molecular Weight:294.781
Hs Code.:

Synonyms:1-(2,4-dimethoxyphenyl)-1-(6-methylpyridin-2-yl)methanamine hydrochloride

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Chemical Property of 1-(2,4-dimethoxyphenyl)-1-(6-methylpyridin-2-yl)methanamine hydrochloride

Chemical Property:

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Technology Process of 1-(2,4-dimethoxyphenyl)-1-(6-methylpyridin-2-yl)methanamine hydrochloride

There total 4 articles about 1-(2,4-dimethoxyphenyl)-1-(6-methylpyridin-2-yl)methanamine hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1187993-15-2
N-[(1Z)-(2,4-dimethoxyphenyl)(6-methylpyridin-2-yl)methylene]-2-methylpropane-2-sulfinamide

: 1187993-14-1
1-(2,4-dimethoxyphenyl)-1-(6-methylpyridin-2-yl)methanamine hydrochloride

Guidance literature:: N-[(1Z)-(2,4-dimethoxyphenyl)(6-methylpyridin-2-yl)methylene]-2-methylpropane-2-sulfinamide; With sodium tetrahydroborate; In methanol; at 0 ℃; for 0.75h;

With ammonium chloride; In methanol; water;

With hydrogenchloride; In diethyl ether; dichloromethane; at 20 ℃; for 0.25h;

Reference yield:

: 1187163-23-0
(2,4-Dimethoxyphenyl)(6-methylpyridin-2-yl)methanone

: 1187993-14-1
1-(2,4-dimethoxyphenyl)-1-(6-methylpyridin-2-yl)methanamine hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1.1: titanium(IV) tetraethanolate / tetrahydrofuran / 24 h / 60 °C

2.1: sodium tetrahydroborate / methanol / 0.75 h / 0 °C

2.3: 0.25 h / 20 °C

With titanium(IV) tetraethanolate; sodium tetrahydroborate; In tetrahydrofuran; methanol;

Reference yield:

: 1620-75-3
2-Cyano-6-methylpyridine

: 1187993-14-1
1-(2,4-dimethoxyphenyl)-1-(6-methylpyridin-2-yl)methanamine hydrochloride

Guidance literature:: Multi-step reaction with 3 steps

1.1: tetrahydrofuran / 3 h / 0 - 20 °C

1.3: pH 10 / Alkaline conditions

2.1: titanium(IV) tetraethanolate / tetrahydrofuran / 24 h / 60 °C

3.1: sodium tetrahydroborate / methanol / 0.75 h / 0 °C

3.3: 0.25 h / 20 °C

With titanium(IV) tetraethanolate; sodium tetrahydroborate; In tetrahydrofuran; methanol;