3-methyl>-N-<(R)-3-(benzyloxy)tetradecanoyl>amino>propyl 2-amino-4,6-O-benzylidene-2-N-<(R)-3-(benzyloxy)tetrdecanoyl>-2-deoxy-β-D-glucopyranoside

Base Information

Chemical Name:3-methyl>-N-<(R)-3-(benzyloxy)tetradecanoyl>amino>propyl 2-amino-4,6-O-benzylidene-2-N-<(R)-3-(benzyloxy)tetrdecanoyl>-2-deoxy-β-D-glucopyranoside
CAS No.:142981-96-2
Molecular Formula:C₆₇H₉₆N₂O₁₁
Molecular Weight:1105.51
Hs Code.:

3-<N-<<(benzyloxy)carbonyl>methyl>-N-<(R)-3-(benzyloxy)tetradecanoyl>amino>propyl 2-amino-4,6-O-benzylidene-2-N-<(R)-3-(benzyloxy)tetrdecanoyl>-2-deoxy-β-D-glucopyranoside

Synonyms:3-methyl>-N-<(R)-3-(benzyloxy)tetradecanoyl>amino>propyl 2-amino-4,6-O-benzylidene-2-N-<(R)-3-(benzyloxy)tetrdecanoyl>-2-deoxy-β-D-glucopyranoside

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Chemical Property of 3-methyl>-N-<(R)-3-(benzyloxy)tetradecanoyl>amino>propyl 2-amino-4,6-O-benzylidene-2-N-<(R)-3-(benzyloxy)tetrdecanoyl>-2-deoxy-β-D-glucopyranoside

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Technology Process of 3-methyl>-N-<(R)-3-(benzyloxy)tetradecanoyl>amino>propyl 2-amino-4,6-O-benzylidene-2-N-<(R)-3-(benzyloxy)tetrdecanoyl>-2-deoxy-β-D-glucopyranoside

There total 6 articles about 3-methyl>-N-<(R)-3-(benzyloxy)tetradecanoyl>amino>propyl 2-amino-4,6-O-benzylidene-2-N-<(R)-3-(benzyloxy)tetrdecanoyl>-2-deoxy-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: 1125-88-8
benzaldehyde dimethyl acetal

: 142981-95-1
3--N-<<(benzyloxy)carbonyl>methyl>amino>propyl 2-amino-2-N-<(R)-3-(benzyloxy)tetradecanoyl>-2-deoxy-β-D-glucopyranoside

: 142981-96-2
3-methyl>-N-<(R)-3-(benzyloxy)tetradecanoyl>amino>propyl 2-amino-4,6-O-benzylidene-2-N-<(R)-3-(benzyloxy)tetrdecanoyl>-2-deoxy-β-D-glucopyranoside

Guidance literature:: With toluene-4-sulfonic acid; In N,N-dimethyl-formamide; at 75 ℃; for 1.5h;
DOI:10.1021/jm00097a003

Reference yield:

: 100-39-0
benzyl bromide

: 142981-96-2
3-methyl>-N-<(R)-3-(benzyloxy)tetradecanoyl>amino>propyl 2-amino-4,6-O-benzylidene-2-N-<(R)-3-(benzyloxy)tetrdecanoyl>-2-deoxy-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) KOH, water, 2.) 20percent aq. Cs₂CO₃

2: 52 percent / p-toluenesulfonic acid monohydrate / dimethylformamide / 1.5 h / 75 °C

With potassium hydroxide; water; caesium carbonate; toluene-4-sulfonic acid; In N,N-dimethyl-formamide;
DOI:10.1021/jm00097a003

Reference yield:

: 101649-06-3
N-((R)-3-Benzyloxytetradecanoyloxy)succinimid

: 142981-96-2
3-methyl>-N-<(R)-3-(benzyloxy)tetradecanoyl>amino>propyl 2-amino-4,6-O-benzylidene-2-N-<(R)-3-(benzyloxy)tetrdecanoyl>-2-deoxy-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 5 steps

1: 30 percent / N-ethyldiisopropylamine / dimethylformamide / 24 h / Ambient temperature

2: 22 percent / anhyd. FeCl₃, drierite / CH₂Cl₂ / 44 h

3: 89 percent / NaOMe / methanol / 22 h / Ambient temperature

4: 1.) KOH, water, 2.) 20percent aq. Cs₂CO₃

5: 52 percent / p-toluenesulfonic acid monohydrate / dimethylformamide / 1.5 h / 75 °C

With calcium sulfate; potassium hydroxide; water; sodium methylate; iron(III) chloride; caesium carbonate; toluene-4-sulfonic acid; N-ethyl-N,N-diisopropylamine; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm00097a003