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methyl P-octyl-N-phenylphosphonamidate

Base Information
  • Chemical Name:methyl P-octyl-N-phenylphosphonamidate
  • CAS No.:1262801-04-6
  • Molecular Formula:C15H26NO2P
  • Molecular Weight:283.351
  • Hs Code.:
methyl P-octyl-N-phenylphosphonamidate

Synonyms:methyl P-octyl-N-phenylphosphonamidate

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Chemical Property of methyl P-octyl-N-phenylphosphonamidate
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Technology Process of methyl P-octyl-N-phenylphosphonamidate

There total 4 articles about methyl P-octyl-N-phenylphosphonamidate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
Phenyl azide; n-octylphosphinic acid methyl ester; With bis-(trimethylsilyl)acetamide; In acetonitrile; at 20 ℃;
With tetrabutyl ammonium fluoride; In acetonitrile; at 20 ℃; for 0.5h;
DOI:10.1039/c0cc02472d
Guidance literature:
Multi-step reaction with 3 steps
1.1: sodium dihydrogen phosphate monohydrate; triethyl borane / methanol / 2 h / 20 °C
2.1: pyridine / dichloromethane / 0.25 h / Reflux
3.1: bis-(trimethylsilyl)acetamide / acetonitrile / 20 °C
3.2: 0.5 h / 20 °C
With pyridine; sodium dihydrogen phosphate monohydrate; triethyl borane; bis-(trimethylsilyl)acetamide; In methanol; dichloromethane; acetonitrile; 3.1: Staudinger reaction;
DOI:10.1039/c0cc02472d
Guidance literature:
Multi-step reaction with 2 steps
1.1: pyridine / dichloromethane / 0.25 h / Reflux
2.1: bis-(trimethylsilyl)acetamide / acetonitrile / 20 °C
2.2: 0.5 h / 20 °C
With pyridine; bis-(trimethylsilyl)acetamide; In dichloromethane; acetonitrile; 2.1: Staudinger reaction;
DOI:10.1039/c0cc02472d
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