(E)-3-(2,4-dichlorophenyl)-1-(4-(2-(2,4-difluorophenyl)-2-methoxy-3-(1H-1,2,4-triazol-1-yl)propoxy)phenyl)prop-2-en-1-one

Base Information

Chemical Name:(E)-3-(2,4-dichlorophenyl)-1-(4-(2-(2,4-difluorophenyl)-2-methoxy-3-(1H-1,2,4-triazol-1-yl)propoxy)phenyl)prop-2-en-1-one
CAS No.:1416163-87-5
Molecular Formula:C₂₇H₂₁Cl₂F₂N₃O₃
Molecular Weight:544.385
Hs Code.:

Synonyms:(E)-3-(2,4-dichlorophenyl)-1-(4-(2-(2,4-difluorophenyl)-2-methoxy-3-(1H-1,2,4-triazol-1-yl)propoxy)phenyl)prop-2-en-1-one

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Chemical Property of (E)-3-(2,4-dichlorophenyl)-1-(4-(2-(2,4-difluorophenyl)-2-methoxy-3-(1H-1,2,4-triazol-1-yl)propoxy)phenyl)prop-2-en-1-one

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Technology Process of (E)-3-(2,4-dichlorophenyl)-1-(4-(2-(2,4-difluorophenyl)-2-methoxy-3-(1H-1,2,4-triazol-1-yl)propoxy)phenyl)prop-2-en-1-one

There total 5 articles about (E)-3-(2,4-dichlorophenyl)-1-(4-(2-(2,4-difluorophenyl)-2-methoxy-3-(1H-1,2,4-triazol-1-yl)propoxy)phenyl)prop-2-en-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.7%

: 1416163-69-3
(E)-3-(2,4-dichlorophenyl)-1-(4-(2-(2,4-difluorophenyl)-2-hydroxy-3-(1H-1,2,4-triazol-1-yl)propoxy)phenyl)prop-2-en-1-one

: 74-88-4
methyl iodide

: 1416163-87-5
(E)-3-(2,4-dichlorophenyl)-1-(4-(2-(2,4-difluorophenyl)-2-methoxy-3-(1H-1,2,4-triazol-1-yl)propoxy)phenyl)prop-2-en-1-one

Guidance literature:: With sodium hydride; In Pionier 2076; N,N-dimethyl-formamide; at 0 - 20 ℃; for 8h; Inert atmosphere;

Reference yield:

: 86386-76-7,123632-22-4,141113-42-0,150024-48-9
1-[2-(2,4-difluorophenyl)-2,3-epoxypropyl]-1H-1,2,4-triazole

: 1416163-87-5
(E)-3-(2,4-dichlorophenyl)-1-(4-(2-(2,4-difluorophenyl)-2-methoxy-3-(1H-1,2,4-triazol-1-yl)propoxy)phenyl)prop-2-en-1-one

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate; tetrabutylammomium bromide / ethyl acetate / 12 h / Reflux; Inert atmosphere

2: sodium hydride / N,N-dimethyl-formamide; Pionier 2076 / 8 h / 0 - 20 °C / Inert atmosphere

With tetrabutylammomium bromide; sodium hydride; potassium carbonate; In Pionier 2076; ethyl acetate; N,N-dimethyl-formamide;

Reference yield:

: 142531-17-7
(E)-1-(4-hydroxyphenyl)-3-(2,4-dichlorophenyl)prop-2-en-1-one

: 1416163-87-5
(E)-3-(2,4-dichlorophenyl)-1-(4-(2-(2,4-difluorophenyl)-2-methoxy-3-(1H-1,2,4-triazol-1-yl)propoxy)phenyl)prop-2-en-1-one

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate; tetrabutylammomium bromide / ethyl acetate / 12 h / Reflux; Inert atmosphere

2: sodium hydride / N,N-dimethyl-formamide; Pionier 2076 / 8 h / 0 - 20 °C / Inert atmosphere

With tetrabutylammomium bromide; sodium hydride; potassium carbonate; In Pionier 2076; ethyl acetate; N,N-dimethyl-formamide;