N,N-diethyl-1-methyl-1-phenylsilylamine

Base Information

Chemical Name:N,N-diethyl-1-methyl-1-phenylsilylamine
CAS No.:134077-65-9
Molecular Formula:C₁₁H₁₉NSi
Molecular Weight:193.364
Hs Code.:

Synonyms:N,N-diethyl-1-methyl-1-phenylsilylamine

Suppliers and Price of N,N-diethyl-1-methyl-1-phenylsilylamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N,N-diethyl-1-methyl-1-phenylsilylamine

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Technology Process of N,N-diethyl-1-methyl-1-phenylsilylamine

There total 2 articles about N,N-diethyl-1-methyl-1-phenylsilylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 766-08-5,146088-00-8
methylphenylsilane

: 109-89-7
diethylamine

: 134077-65-9
N,N-diethyl-1-methyl-1-phenylsilylamine

Guidance literature:: With C₃₆H₇₀N₈O₂Si₄Y₂; In toluene; at 20 ℃; for 0.25h; Glovebox; Schlenk technique;
DOI:10.1021/acs.inorgchem.0c00907

Reference yield:

: 149-74-6
dichloromethylphenylsilane

: 134077-65-9
N,N-diethyl-1-methyl-1-phenylsilylamine

Guidance literature:: Multi-step reaction with 2 steps

1: 79 percent / diethyl ether / 2 h / Heating

2: 58 percent / LiAlH₄ / tetrahydrofuran / 4 h / Heating

With lithium aluminium tetrahydride; In tetrahydrofuran; diethyl ether;
DOI:10.1139/v00-025