3-amino-5-(3,5-dimethylisoxazol-4-yl)-1-(4-morpholinobenzyl)pyridin-2(1H)-one

Base Information

Chemical Name:3-amino-5-(3,5-dimethylisoxazol-4-yl)-1-(4-morpholinobenzyl)pyridin-2(1H)-one
CAS No.:1616402-39-1
Molecular Formula:C₂₁H₂₄N₄O₃
Molecular Weight:380.447
Hs Code.:

Synonyms:3-amino-5-(3,5-dimethylisoxazol-4-yl)-1-(4-morpholinobenzyl)pyridin-2(1H)-one

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Chemical Property of 3-amino-5-(3,5-dimethylisoxazol-4-yl)-1-(4-morpholinobenzyl)pyridin-2(1H)-one

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Technology Process of 3-amino-5-(3,5-dimethylisoxazol-4-yl)-1-(4-morpholinobenzyl)pyridin-2(1H)-one

There total 7 articles about 3-amino-5-(3,5-dimethylisoxazol-4-yl)-1-(4-morpholinobenzyl)pyridin-2(1H)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 1616403-03-2
C₂₃H₂₆N₄O₄

: 1616402-39-1
3-amino-5-(3,5-dimethylisoxazol-4-yl)-1-(4-morpholinobenzyl)pyridin-2(1H)-one

Guidance literature:: With water; lithium hydroxide; In 1,4-dioxane; at 100 ℃; for 17h; Inert atmosphere;

Reference yield:

: 1616402-83-5
C₁₀H₁₁N₃O₂

: 1616402-39-1
3-amino-5-(3,5-dimethylisoxazol-4-yl)-1-(4-morpholinobenzyl)pyridin-2(1H)-one

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine / dichloromethane / 17 h / 20 °C

2: potassium carbonate / acetonitrile / 17 h / 60 °C

3: lithium hydroxide; water / 1,4-dioxane / 17 h / 100 °C / Inert atmosphere

With water; potassium carbonate; triethylamine; lithium hydroxide; In 1,4-dioxane; dichloromethane; acetonitrile;

Reference yield:

: 1616402-82-4
C₁₁H₁₃N₃O₂

: 1616402-39-1
3-amino-5-(3,5-dimethylisoxazol-4-yl)-1-(4-morpholinobenzyl)pyridin-2(1H)-one

Guidance literature:: Multi-step reaction with 4 steps

1: hydrogen bromide / 1 h / 85 °C

2: triethylamine / dichloromethane / 17 h / 20 °C

3: potassium carbonate / acetonitrile / 17 h / 60 °C

4: lithium hydroxide; water / 1,4-dioxane / 17 h / 100 °C / Inert atmosphere

With water; hydrogen bromide; potassium carbonate; triethylamine; lithium hydroxide; In 1,4-dioxane; dichloromethane; acetonitrile;