potassium salt of N-[2-(3-sulfopropoxy)phenyl]-1,8-naphthalimide

Base Information

Chemical Name:potassium salt of N-[2-(3-sulfopropoxy)phenyl]-1,8-naphthalimide
CAS No.:1335138-05-0
Molecular Formula:C₂₁H₁₆NO₆S*K
Molecular Weight:449.525
Hs Code.:

Synonyms:potassium salt of N-[2-(3-sulfopropoxy)phenyl]-1,8-naphthalimide

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Chemical Property of potassium salt of N-[2-(3-sulfopropoxy)phenyl]-1,8-naphthalimide

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Technology Process of potassium salt of N-[2-(3-sulfopropoxy)phenyl]-1,8-naphthalimide

There total 3 articles about potassium salt of N-[2-(3-sulfopropoxy)phenyl]-1,8-naphthalimide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 1120-71-4
1,3-propanesultone

: 6917-30-2
2-(2-hydroxyphenyl)-1H-benzo[de]isoquinoline-1,3(2H)- dione

: 1335138-05-0
potassium salt of N-[2-(3-sulfopropoxy)phenyl]-1,8-naphthalimide

Guidance literature:: 2-(2-hydroxyphenyl)-1H-benzo[de]isoquinoline-1,3(2H)- dione; With potassium carbonate; In N,N-dimethyl-formamide; for 0.5h;

1,3-propanesultone; In N,N-dimethyl-formamide; at 20 ℃; for 8h;
DOI:10.1007/s11172-011-0080-4

Reference yield:

: 81-84-5
1,8-Naphthalic anhydride

: 1335138-05-0
potassium salt of N-[2-(3-sulfopropoxy)phenyl]-1,8-naphthalimide

Guidance literature:: Multi-step reaction with 2 steps

1.1: triethylamine; benzoic acid / N,N-dimethyl-formamide / 12 h / 70 °C

2.1: potassium carbonate / N,N-dimethyl-formamide / 0.5 h

2.2: 8 h / 20 °C

With potassium carbonate; triethylamine; benzoic acid; In N,N-dimethyl-formamide;
DOI:10.1007/s11172-011-0080-4

Reference yield:

: 95-55-6
2-amino-phenol

: 1335138-05-0
potassium salt of N-[2-(3-sulfopropoxy)phenyl]-1,8-naphthalimide

Guidance literature:: Multi-step reaction with 2 steps

1.1: triethylamine; benzoic acid / N,N-dimethyl-formamide / 12 h / 70 °C

2.1: potassium carbonate / N,N-dimethyl-formamide / 0.5 h

2.2: 8 h / 20 °C

With potassium carbonate; triethylamine; benzoic acid; In N,N-dimethyl-formamide;
DOI:10.1007/s11172-011-0080-4