11-tritylsulfanyl-undecanoic acid {2-[2-(2-amino-ethoxy)-ethoxy]-ethyl}-amide

Base Information

Chemical Name:11-tritylsulfanyl-undecanoic acid {2-[2-(2-amino-ethoxy)-ethoxy]-ethyl}-amide
CAS No.:792921-26-7
Molecular Formula:C₃₆H₅₀N₂O₃S
Molecular Weight:590.871
Hs Code.:

Synonyms:11-tritylsulfanyl-undecanoic acid {2-[2-(2-amino-ethoxy)-ethoxy]-ethyl}-amide

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Chemical Property of 11-tritylsulfanyl-undecanoic acid {2-[2-(2-amino-ethoxy)-ethoxy]-ethyl}-amide

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Technology Process of 11-tritylsulfanyl-undecanoic acid {2-[2-(2-amino-ethoxy)-ethoxy]-ethyl}-amide

There total 4 articles about 11-tritylsulfanyl-undecanoic acid {2-[2-(2-amino-ethoxy)-ethoxy]-ethyl}-amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 929-59-9,892154-56-2
3,6-dioxa-1,8-diaminooctane

: 916980-32-0
C₃₄H₃₉NO₄S

: 792921-26-7
11-tritylsulfanyl-undecanoic acid {2-[2-(2-amino-ethoxy)-ethoxy]-ethyl}-amide

Guidance literature:: In dichloromethane; at 20 ℃; for 12h;

Reference yield:

: 202462-83-7
11-[(triphenylmethyl)sulfanyl]undecanoic Acid

: 792921-26-7
11-tritylsulfanyl-undecanoic acid {2-[2-(2-amino-ethoxy)-ethoxy]-ethyl}-amide

Guidance literature:: Multi-step reaction with 2 steps

1: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 13 h / 5 - 20 °C

2: dichloromethane / 20 °C

With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane;
DOI:10.1002/anie.201008198

Reference yield:

: 71310-21-9
11-mercaptounadecanoic acid

: 792921-26-7
11-tritylsulfanyl-undecanoic acid {2-[2-(2-amino-ethoxy)-ethoxy]-ethyl}-amide

Guidance literature:: Multi-step reaction with 3 steps

1: N-ethyl-N,N-diisopropylamine / toluene / 3 h / 20 °C

2: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 13 h / 5 - 20 °C

3: dichloromethane / 20 °C

With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; In dichloromethane; toluene;
DOI:10.1002/anie.201008198