3-methoxy-4-[13-(2-methoxyphenyl)-1,4,10-trioxa-7,13-diazacyclopentadecan-7-yl]phenylamine

Base Information

Chemical Name:3-methoxy-4-[13-(2-methoxyphenyl)-1,4,10-trioxa-7,13-diazacyclopentadecan-7-yl]phenylamine
CAS No.:497969-01-4
Molecular Formula:C₂₄H₃₅N₃O₅
Molecular Weight:445.559
Hs Code.:

Synonyms:3-methoxy-4-[13-(2-methoxyphenyl)-1,4,10-trioxa-7,13-diazacyclopentadecan-7-yl]phenylamine

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Chemical Property of 3-methoxy-4-[13-(2-methoxyphenyl)-1,4,10-trioxa-7,13-diazacyclopentadecan-7-yl]phenylamine

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Technology Process of 3-methoxy-4-[13-(2-methoxyphenyl)-1,4,10-trioxa-7,13-diazacyclopentadecan-7-yl]phenylamine

There total 8 articles about 3-methoxy-4-[13-(2-methoxyphenyl)-1,4,10-trioxa-7,13-diazacyclopentadecan-7-yl]phenylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

: 497968-89-5
7-(2-methoxy-4-nitrophenyl)-13-(2-methoxyphenyl)-1,4,10-trioxa-7,13-diazacyclopentadecane

: 497969-01-4
3-methoxy-4-[13-(2-methoxyphenyl)-1,4,10-trioxa-7,13-diazacyclopentadecan-7-yl]phenylamine

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethanol;
DOI:10.1039/b205299g

Reference yield:

: 6295-94-9
N-tosyl-2-anisidine

: 497969-01-4
3-methoxy-4-[13-(2-methoxyphenyl)-1,4,10-trioxa-7,13-diazacyclopentadecan-7-yl]phenylamine

Guidance literature:: Multi-step reaction with 6 steps

1: 90.76 percent / K₂CO₃; KI / dimethylformamide / 72 h / 70 °C

2: 31.6 percent / H₂SO₄ / acetic acid / 24 h / 60 °C

3: 67 percent / pyridine / benzene / 12 h / 75 °C

4: 97.67 percent / NaBH₄; BF₃*Et₂O / tetrahydrofuran / 4 h / Heating

5: 48 percent / glacial acetic acid; aq. NaNO₂ / 20 °C

6: 59 percent / H₂ / 10 percent Pd/C / ethanol

With pyridine; sodium tetrahydroborate; sulfuric acid; boron trifluoride diethyl etherate; hydrogen; potassium carbonate; acetic acid; potassium iodide; sodium nitrite; palladium on activated charcoal; In tetrahydrofuran; ethanol; acetic acid; N,N-dimethyl-formamide; benzene;
DOI:10.1039/b205299g

Reference yield:

: 497968-92-0
1,10-bis(2-methoxyphenyl)-4,7-dioxa-1,10-diazadecane

: 497969-01-4
3-methoxy-4-[13-(2-methoxyphenyl)-1,4,10-trioxa-7,13-diazacyclopentadecan-7-yl]phenylamine

Guidance literature:: Multi-step reaction with 4 steps

1: 67 percent / pyridine / benzene / 12 h / 75 °C

2: 97.67 percent / NaBH₄; BF₃*Et₂O / tetrahydrofuran / 4 h / Heating

3: 48 percent / glacial acetic acid; aq. NaNO₂ / 20 °C

4: 59 percent / H₂ / 10 percent Pd/C / ethanol

With pyridine; sodium tetrahydroborate; boron trifluoride diethyl etherate; hydrogen; acetic acid; sodium nitrite; palladium on activated charcoal; In tetrahydrofuran; ethanol; benzene;
DOI:10.1039/b205299g