1-(tert-buty-dimethyl-silanyloxy)-3-iodo-6,6-dimethyl-cyclohex-2-enecarbonitrile

Base Information

Chemical Name:1-(tert-buty-dimethyl-silanyloxy)-3-iodo-6,6-dimethyl-cyclohex-2-enecarbonitrile
CAS No.:1020202-93-0
Molecular Formula:C₁₅H₂₆INOSi
Molecular Weight:391.368
Hs Code.:

Synonyms:1-(tert-buty-dimethyl-silanyloxy)-3-iodo-6,6-dimethyl-cyclohex-2-enecarbonitrile

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-(tert-buty-dimethyl-silanyloxy)-3-iodo-6,6-dimethyl-cyclohex-2-enecarbonitrile

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Technology Process of 1-(tert-buty-dimethyl-silanyloxy)-3-iodo-6,6-dimethyl-cyclohex-2-enecarbonitrile

There total 1 articles about 1-(tert-buty-dimethyl-silanyloxy)-3-iodo-6,6-dimethyl-cyclohex-2-enecarbonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 1020202-99-6
3-iodo-6,6-dimethyl-cyclohex-2-enone

: 56522-24-8
tert-butyldimethylsilyl cyanide

: 1020202-93-0
1-(tert-buty-dimethyl-silanyloxy)-3-iodo-6,6-dimethyl-cyclohex-2-enecarbonitrile

Guidance literature:: With zinc(II) iodide; In acetonitrile; at 20 ℃; for 24h;
DOI:10.1021/ol800429j

Reference yield: 76.0%

: 1020202-65-6
1-(2-azido-phenyl)-prop-2-ynyl acetate

: 1020202-93-0
1-(tert-buty-dimethyl-silanyloxy)-3-iodo-6,6-dimethyl-cyclohex-2-enecarbonitrile

: 1020202-97-4
acetic acid 1-(2-azido-phenyl)-3-[3-(tert-butyl-dimethyl-silanyloxy)-3-cyano-4,4-dimethyl-cyclohex-1-enyl]-prop-2-ynyl ester

Guidance literature:: With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine; In tetrahydrofuran; for 16h; Inert atmosphere;
DOI:10.1021/ol800429j