acetic acid 1-(2-azido-phenyl)-3-[3-(tert-butyl-dimethyl-silanyloxy)-3-cyano-4,4-dimethyl-cyclohex-1-enyl]-prop-2-ynyl ester

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Chemical Name:acetic acid 1-(2-azido-phenyl)-3-[3-(tert-butyl-dimethyl-silanyloxy)-3-cyano-4,4-dimethyl-cyclohex-1-enyl]-prop-2-ynyl ester
CAS No.:1020202-97-4
Molecular Formula:C₂₆H₃₄N₄O₃Si
Molecular Weight:478.666
Hs Code.:

Synonyms:acetic acid 1-(2-azido-phenyl)-3-[3-(tert-butyl-dimethyl-silanyloxy)-3-cyano-4,4-dimethyl-cyclohex-1-enyl]-prop-2-ynyl ester

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Chemical Property of acetic acid 1-(2-azido-phenyl)-3-[3-(tert-butyl-dimethyl-silanyloxy)-3-cyano-4,4-dimethyl-cyclohex-1-enyl]-prop-2-ynyl ester

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Technology Process of acetic acid 1-(2-azido-phenyl)-3-[3-(tert-butyl-dimethyl-silanyloxy)-3-cyano-4,4-dimethyl-cyclohex-1-enyl]-prop-2-ynyl ester

There total 1 articles about acetic acid 1-(2-azido-phenyl)-3-[3-(tert-butyl-dimethyl-silanyloxy)-3-cyano-4,4-dimethyl-cyclohex-1-enyl]-prop-2-ynyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 1020202-65-6
1-(2-azido-phenyl)-prop-2-ynyl acetate

: 1020202-93-0
1-(tert-buty-dimethyl-silanyloxy)-3-iodo-6,6-dimethyl-cyclohex-2-enecarbonitrile

: 1020202-97-4
acetic acid 1-(2-azido-phenyl)-3-[3-(tert-butyl-dimethyl-silanyloxy)-3-cyano-4,4-dimethyl-cyclohex-1-enyl]-prop-2-ynyl ester

Guidance literature:: With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine; In tetrahydrofuran; for 16h; Inert atmosphere;
DOI:10.1021/ol800429j

Reference yield: 81.0%

: 1020202-97-4
acetic acid 1-(2-azido-phenyl)-3-[3-(tert-butyl-dimethyl-silanyloxy)-3-cyano-4,4-dimethyl-cyclohex-1-enyl]-prop-2-ynyl ester

: 75-16-1
methylmagnesium bromide

: 1020202-77-0
3-[3-(2-azido-phenyl)-1-methyl-propa-1,2-dienyl]-1-(tert-butyl-dimethyl-silanyloxy)-6,6-dimethyl-cyclohex-2-enecarbonitrile

Guidance literature:: methylmagnesium bromide; With copper(l) iodide; lithium bromide; In tetrahydrofuran; diethyl ether; for 0.5h; Cooling with ice;

acetic acid 1-(2-azido-phenyl)-3-[3-(tert-butyl-dimethyl-silanyloxy)-3-cyano-4,4-dimethyl-cyclohex-1-enyl]-prop-2-ynyl ester; In tetrahydrofuran; diethyl ether; for 0.5h; Cooling with ice;

With water; ammonium chloride; In tetrahydrofuran; diethyl ether; Cooling with ice;
DOI:10.1021/ol800429j