Technology Process of C24H31FN2O2Si
There total 5 articles about C24H31FN2O2Si which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
palladium 10% on activated carbon; ammonium formate;
In
tetrahydrofuran; methanol;
at 20 ℃;
for 1h;
Inert atmosphere;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 16 h / 20 °C / Cooling with ice
2: ammonium formate; palladium 10% on activated carbon / methanol; tetrahydrofuran / 1 h / 20 °C / Inert atmosphere
With
di-isopropyl azodicarboxylate; palladium 10% on activated carbon; ammonium formate; triphenylphosphine;
In
tetrahydrofuran; methanol;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: tetrakis(triphenylphosphine) palladium(0); sodium carbonate / water; 1,2-dimethoxyethane / 16 h / 90 °C / Inert atmosphere
2: 2-(methylsulfonyl)ethyl alcohol; sodium hydride / N,N-dimethyl-formamide; mineral oil / 2 h / 20 °C
3: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 16 h / 20 °C / Cooling with ice
4: ammonium formate; palladium 10% on activated carbon / methanol; tetrahydrofuran / 1 h / 20 °C / Inert atmosphere
With
tetrakis(triphenylphosphine) palladium(0); 2-(methylsulfonyl)ethyl alcohol; di-isopropyl azodicarboxylate; palladium 10% on activated carbon; ammonium formate; sodium hydride; sodium carbonate; triphenylphosphine;
In
tetrahydrofuran; methanol; 1,2-dimethoxyethane; water; N,N-dimethyl-formamide; mineral oil;