N-[[2-chloro-4-[2-(3,5-dichlorophenyl)-2-(trifluoromethyl)-3H-furan-4-yl]phenyl]methyl]-2-ethylbutanamide

Base Information

Chemical Name:N-[[2-chloro-4-[2-(3,5-dichlorophenyl)-2-(trifluoromethyl)-3H-furan-4-yl]phenyl]methyl]-2-ethylbutanamide
CAS No.:1425942-39-7
Molecular Formula:C₂₄H₂₃Cl₃F₃NO₂
Molecular Weight:520.806
Hs Code.:

Synonyms:N-[[2-chloro-4-[2-(3,5-dichlorophenyl)-2-(trifluoromethyl)-3H-furan-4-yl]phenyl]methyl]-2-ethylbutanamide

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Chemical Property of N-[[2-chloro-4-[2-(3,5-dichlorophenyl)-2-(trifluoromethyl)-3H-furan-4-yl]phenyl]methyl]-2-ethylbutanamide

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Technology Process of N-[[2-chloro-4-[2-(3,5-dichlorophenyl)-2-(trifluoromethyl)-3H-furan-4-yl]phenyl]methyl]-2-ethylbutanamide

There total 6 articles about N-[[2-chloro-4-[2-(3,5-dichlorophenyl)-2-(trifluoromethyl)-3H-furan-4-yl]phenyl]methyl]-2-ethylbutanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1425942-92-2
[2-chloro-4-[2-(3,5-dichlorophenyl)-2-(trifluoromethyl)-3H-furan-4-yl]phenyl]methanamine

: 1425942-39-7
N-[[2-chloro-4-[2-(3,5-dichlorophenyl)-2-(trifluoromethyl)-3H-furan-4-yl]phenyl]methyl]-2-ethylbutanamide

Guidance literature:: In N,N-dimethyl acetamide; for 16h;

Reference yield:

: 1425942-96-6
2-[[2-chloro-4-[(E)-3-(3,5-dichlorophenyl)-4,4,4-trifluoro-3-hydroxy-but-1-enyl]phenyl]methyl]isoindoline-1,3-dione

: 1425942-39-7
N-[[2-chloro-4-[2-(3,5-dichlorophenyl)-2-(trifluoromethyl)-3H-furan-4-yl]phenyl]methyl]-2-ethylbutanamide

Guidance literature:: Multi-step reaction with 4 steps

1: dicarbonylacetylacetonato rhodium (I); tris(2,4-di-tert-butylphenyl)phosphite; hydrogen / tetrahydrofuran / 36 h / 100 °C / 37503.8 Torr / Inert atmosphere

2: toluene-4-sulfonic acid / 5,5-dimethyl-1,3-cyclohexadiene / 2 h / 130 °C / Inert atmosphere

3: hydrazine hydrate / ethanol / 0.33 h / 80 °C

4: N,N-dimethyl acetamide / 16 h

With dicarbonylacetylacetonato rhodium (I); tris(2,4-di-tert-butylphenyl)phosphite; hydrogen; toluene-4-sulfonic acid; hydrazine hydrate; In tetrahydrofuran; 5,5-dimethyl-1,3-cyclohexadiene; ethanol; N,N-dimethyl acetamide;

Reference yield:

: 1425942-97-7
2-[[2-chloro-4-[5-(3,5-dichlorophenyl)-2-hydroxy-5-(trifluoromethyl)tetrahydrofuran-3-yl]phenyl]methyl]isoindoline-1,3-dione

: 1425942-39-7
N-[[2-chloro-4-[2-(3,5-dichlorophenyl)-2-(trifluoromethyl)-3H-furan-4-yl]phenyl]methyl]-2-ethylbutanamide

Guidance literature:: Multi-step reaction with 3 steps

1: toluene-4-sulfonic acid / 5,5-dimethyl-1,3-cyclohexadiene / 2 h / 130 °C / Inert atmosphere

2: hydrazine hydrate / ethanol / 0.33 h / 80 °C

3: N,N-dimethyl acetamide / 16 h

With toluene-4-sulfonic acid; hydrazine hydrate; In 5,5-dimethyl-1,3-cyclohexadiene; ethanol; N,N-dimethyl acetamide;