(S)-3-(3-Acetyl-5-iodo-4-methoxy-phenyl)-2-benzyloxycarbonylamino-propionic acid methyl ester

Base Information

Chemical Name:(S)-3-(3-Acetyl-5-iodo-4-methoxy-phenyl)-2-benzyloxycarbonylamino-propionic acid methyl ester
CAS No.:851915-13-4
Molecular Formula:C₂₁H₂₂INO₆
Molecular Weight:511.313
Hs Code.:

Synonyms:(S)-3-(3-Acetyl-5-iodo-4-methoxy-phenyl)-2-benzyloxycarbonylamino-propionic acid methyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-3-(3-Acetyl-5-iodo-4-methoxy-phenyl)-2-benzyloxycarbonylamino-propionic acid methyl ester

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Technology Process of (S)-3-(3-Acetyl-5-iodo-4-methoxy-phenyl)-2-benzyloxycarbonylamino-propionic acid methyl ester

There total 1 articles about (S)-3-(3-Acetyl-5-iodo-4-methoxy-phenyl)-2-benzyloxycarbonylamino-propionic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1150635-46-3
L-N-Cbz-3-acetyl-5-iodotyrosine methyl ester

: 74-88-4
methyl iodide

: 851915-13-4
(S)-3-(3-Acetyl-5-iodo-4-methoxy-phenyl)-2-benzyloxycarbonylamino-propionic acid methyl ester

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 20 ℃;
DOI:10.1055/s-0028-1087548

Reference yield: 85.0%

: 851915-13-4
(S)-3-(3-Acetyl-5-iodo-4-methoxy-phenyl)-2-benzyloxycarbonylamino-propionic acid methyl ester

: 823-96-1
Trimethylboroxine

: 1150635-56-5
C₂₂H₂₅NO₆

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; 2,6-di-tert-butyl-4-methyl-phenol; potassium carbonate; In 1,4-dioxane; at 100 ℃; for 2h; Microwave irradiation; Inert atmosphere;
DOI:10.1055/s-0028-1087548

Reference yield: 40.0%

: 851915-13-4
(S)-3-(3-Acetyl-5-iodo-4-methoxy-phenyl)-2-benzyloxycarbonylamino-propionic acid methyl ester

: 851914-85-7
2-tert-butoxycarbonylamino-3-(4-methoxymethoxy-3-tributylstannanyl-phenyl)-propionic acid tert-butyl ester

: 3-[5-acetyl-5'-(2-tert-butoxycarbonyl-2-tert-butoxycarbonylamino-ethyl)-6-methoxy-2'-methoxymethoxy-biphenyl-3-yl]-2-benzyloxycarbonylamino-propionic acid methyl ester

Guidance literature:: With copper(l) iodide; triphenyl-arsane; bis-triphenylphosphine-palladium(II) chloride; In 1-methyl-pyrrolidin-2-one; at 100 ℃; for 7h;
DOI:10.1016/j.tetlet.2005.02.078