ethyl N-(3-carbamoyl-3,3-diphenylpropyl)oxamic acid ester

Base Information

Chemical Name:ethyl N-(3-carbamoyl-3,3-diphenylpropyl)oxamic acid ester
CAS No.:503598-82-1
Molecular Formula:C₂₀H₂₂N₂O₄
Molecular Weight:354.406
Hs Code.:

Synonyms:ethyl N-(3-carbamoyl-3,3-diphenylpropyl)oxamic acid ester

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Chemical Property of ethyl N-(3-carbamoyl-3,3-diphenylpropyl)oxamic acid ester

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Technology Process of ethyl N-(3-carbamoyl-3,3-diphenylpropyl)oxamic acid ester

There total 4 articles about ethyl N-(3-carbamoyl-3,3-diphenylpropyl)oxamic acid ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 503598-78-5
4-amino-2-diphenylbutanamide

: 4755-77-5
Ethyl oxalyl chloride

: 503598-82-1
ethyl N-(3-carbamoyl-3,3-diphenylpropyl)oxamic acid ester

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃; for 0.166667h;
DOI:10.1248/cpb.55.1039

Reference yield:

: 503598-74-1
C₃₀H₃₀N₂O

: 503598-82-1
ethyl N-(3-carbamoyl-3,3-diphenylpropyl)oxamic acid ester

Guidance literature:: Multi-step reaction with 2 steps

1: H₂ / Perlman's catalyst

2: 67 percent / Et₃N / CH₂Cl₂ / 0.17 h / 20 °C

With hydrogen; triethylamine; palladium hydroxide - carbon; In dichloromethane;
DOI:10.1248/cpb.55.1039

Reference yield:

: 86-29-3
Diphenylacetonitrile

: 503598-82-1
ethyl N-(3-carbamoyl-3,3-diphenylpropyl)oxamic acid ester

Guidance literature:: Multi-step reaction with 4 steps

1: NaH / dimethylformamide

2: aq. KOH / propan-2-ol

3: H₂ / Perlman's catalyst

4: 67 percent / Et₃N / CH₂Cl₂ / 0.17 h / 20 °C

With potassium hydroxide; hydrogen; sodium hydride; triethylamine; palladium hydroxide - carbon; In dichloromethane; N,N-dimethyl-formamide; isopropyl alcohol;
DOI:10.1248/cpb.55.1039