O-(6-O-Acetyl-2,3,4-tri-O-benzyl-α-D-glucopyranosyl)-(1->6)-1-O-acetyl-2,3,4-tri-O-benzyl-α-D-glucopyranose

Base Information

Chemical Name:O-(6-O-Acetyl-2,3,4-tri-O-benzyl-α-D-glucopyranosyl)-(1->6)-1-O-acetyl-2,3,4-tri-O-benzyl-α-D-glucopyranose
CAS No.:145149-86-6
Molecular Formula:C₅₈H₆₂O₁₃
Molecular Weight:967.122
Hs Code.:

Synonyms:O-(6-O-Acetyl-2,3,4-tri-O-benzyl-α-D-glucopyranosyl)-(1->6)-1-O-acetyl-2,3,4-tri-O-benzyl-α-D-glucopyranose

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Chemical Property of O-(6-O-Acetyl-2,3,4-tri-O-benzyl-α-D-glucopyranosyl)-(1->6)-1-O-acetyl-2,3,4-tri-O-benzyl-α-D-glucopyranose

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Technology Process of O-(6-O-Acetyl-2,3,4-tri-O-benzyl-α-D-glucopyranosyl)-(1->6)-1-O-acetyl-2,3,4-tri-O-benzyl-α-D-glucopyranose

There total 10 articles about O-(6-O-Acetyl-2,3,4-tri-O-benzyl-α-D-glucopyranosyl)-(1->6)-1-O-acetyl-2,3,4-tri-O-benzyl-α-D-glucopyranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 153541-58-3
1-O-acetyl-2,3,4-tri-O-benzyl-α-D-glucopyranoside

: 441017-58-9
6-O-acetyl-2,3,4-tri-O-benzyl-α-D-glucopyranosyl iodide

: 145149-86-6
O-(6-O-Acetyl-2,3,4-tri-O-benzyl-α-D-glucopyranosyl)-(1->6)-1-O-acetyl-2,3,4-tri-O-benzyl-α-D-glucopyranose

Guidance literature:: With tetra-(n-butyl)ammonium iodide; N-ethyl-N,N-diisopropylamine; In benzene; for 3h; Heating;

Reference yield: 61.0%

: 108-24-7
acetic anhydride

: 38184-15-5
methyl 6-O-acetyl-2,3,4-tri-O-benzyl-α-D-glucopyranosyl-(1<*>6)-2,3,4-tri-O-benzyl-α-D-glucopyranoside

: 145149-86-6,145149-87-7
O-(6-O-Acetyl-2,3,4-tri-O-benzyl-α-D-glucopyranosyl)-(1->6)-1-O-acetyl-2,3,4-tri-O-benzyl-α,β-D-glucopyranose

Guidance literature:: With toluene-4-sulfonic acid; at 70 ℃; for 2h; Sealed tube; Inert atmosphere;
DOI:10.1002/anie.201901346

Reference yield:

: 4356-77-8
acetyl 6-O-acetyl-2,3,4-tri-O-benzyl-α-D-glucopyranoside

: 145149-86-6
O-(6-O-Acetyl-2,3,4-tri-O-benzyl-α-D-glucopyranosyl)-(1->6)-1-O-acetyl-2,3,4-tri-O-benzyl-α-D-glucopyranose

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / iodo trimethylsilane / CH₂Cl₂ / 2 h / 0 °C

2: 93 percent / tetrabutylammonium idide; diisopropylethylamine / benzene / 3 h / Heating

With trimethylsilyl iodide; tetra-(n-butyl)ammonium iodide; N-ethyl-N,N-diisopropylamine; In dichloromethane; benzene;