4-(3′,5′-dimethylphenyl)-3-azadibenzothiophene

Base Information

Chemical Name:4-(3′,5′-dimethylphenyl)-3-azadibenzothiophene
CAS No.:1251041-78-7
Molecular Formula:C₁₉H₁₅NS
Molecular Weight:289.401
Hs Code.:

Synonyms:4-(3′,5′-dimethylphenyl)-3-azadibenzothiophene

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Chemical Property of 4-(3′,5′-dimethylphenyl)-3-azadibenzothiophene

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Technology Process of 4-(3′,5′-dimethylphenyl)-3-azadibenzothiophene

There total 5 articles about 4-(3′,5′-dimethylphenyl)-3-azadibenzothiophene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 1-chlorobenzo[4,5]thieno[2,3-c]pyridine

: 172975-69-8
3,5-dimethylphenyl boronic acid

: 1251041-78-7
4-(3′,5′-dimethylphenyl)-3-azadibenzothiophene

Guidance literature:: With dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; potassium phosphate monohydrate; In water; toluene; for 18h; Inert atmosphere; Reflux;

Reference yield:

: 504-29-0
2-aminopyridine

: 1251041-78-7
4-(3′,5′-dimethylphenyl)-3-azadibenzothiophene

Guidance literature:: With tert.-butylnitrite; sodium hydrogencarbonate; In acetic acid;

Reference yield:

: 909036-46-0
2-chloro-3-iodo-pyridin-4-ylamine

: 1251041-78-7
4-(3′,5′-dimethylphenyl)-3-azadibenzothiophene

Guidance literature:: Multi-step reaction with 3 steps

1: ethylene glycol; potassium carbonate; copper(l) iodide / isopropyl alcohol / 18 h / Reflux

2: acetic acid; tert.-butylnitrite / 3.25 h / 20 °C

3: potassium phosphate monohydrate; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane / water; toluene / 18 h / Inert atmosphere; Reflux

With dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; copper(l) iodide; tert.-butylnitrite; potassium phosphate monohydrate; potassium carbonate; ethylene glycol; acetic acid; In water; isopropyl alcohol; toluene;