(S)-2-Benzyloxycarbonylamino-N-((2R,3R,4R,5S,6R)-4,5-diacetoxy-6-acetoxymethyl-3-acetylamino-tetrahydro-pyran-2-yl)-succinamic acid 2-methoxy-ethyl ester

Base Information

Chemical Name:(S)-2-Benzyloxycarbonylamino-N-((2R,3R,4R,5S,6R)-4,5-diacetoxy-6-acetoxymethyl-3-acetylamino-tetrahydro-pyran-2-yl)-succinamic acid 2-methoxy-ethyl ester
CAS No.:202266-11-3
Molecular Formula:C₂₉H₃₉N₃O₁₄
Molecular Weight:653.64
Hs Code.:

(S)-2-Benzyloxycarbonylamino-N-((2R,3R,4R,5S,6R)-4,5-diacetoxy-6-acetoxymethyl-3-acetylamino-tetrahydro-pyran-2-yl)-succinamic acid 2-methoxy-ethyl ester

Synonyms:(S)-2-Benzyloxycarbonylamino-N-((2R,3R,4R,5S,6R)-4,5-diacetoxy-6-acetoxymethyl-3-acetylamino-tetrahydro-pyran-2-yl)-succinamic acid 2-methoxy-ethyl ester

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Chemical Property of (S)-2-Benzyloxycarbonylamino-N-((2R,3R,4R,5S,6R)-4,5-diacetoxy-6-acetoxymethyl-3-acetylamino-tetrahydro-pyran-2-yl)-succinamic acid 2-methoxy-ethyl ester

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Technology Process of (S)-2-Benzyloxycarbonylamino-N-((2R,3R,4R,5S,6R)-4,5-diacetoxy-6-acetoxymethyl-3-acetylamino-tetrahydro-pyran-2-yl)-succinamic acid 2-methoxy-ethyl ester

There total 3 articles about (S)-2-Benzyloxycarbonylamino-N-((2R,3R,4R,5S,6R)-4,5-diacetoxy-6-acetoxymethyl-3-acetylamino-tetrahydro-pyran-2-yl)-succinamic acid 2-methoxy-ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 202266-03-3
bis(2-methoxyethyl) N-benzyloxycarbonyl-L-aspartate

: 202266-11-3
(S)-2-Benzyloxycarbonylamino-N-((2R,3R,4R,5S,6R)-4,5-diacetoxy-6-acetoxymethyl-3-acetylamino-tetrahydro-pyran-2-yl)-succinamic acid 2-methoxy-ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 82 percent / aq. sodium phosphate buffer, lipase A₆ (Amano) / acetone / 1.5 h / 37 °C

2: 1.) isobutyl 2-isobutoxy-1,2-dihydroquinoline-1-carboxylate / 1.) CH₂Cl₂, 15 min, 2.) CH₂Cl₂, 8 h

With 2-isobutoxy-1-isobutoxycarbonyl-1,2-dihydroquinoline; sodium phosphate buffer; lipase A₆ (Amano); In acetone;
DOI:10.1055/s-1997-1374

Reference yield:

: (S)-2-Amino-succinic acid bis-(2-methoxy-ethyl) ester; compound with toluene-4-sulfonic acid

: 202266-11-3
(S)-2-Benzyloxycarbonylamino-N-((2R,3R,4R,5S,6R)-4,5-diacetoxy-6-acetoxymethyl-3-acetylamino-tetrahydro-pyran-2-yl)-succinamic acid 2-methoxy-ethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 80 percent / Et₃N / CH₂Cl₂ / 5 h / Ambient temperature

2: 82 percent / aq. sodium phosphate buffer, lipase A₆ (Amano) / acetone / 1.5 h / 37 °C

3: 1.) isobutyl 2-isobutoxy-1,2-dihydroquinoline-1-carboxylate / 1.) CH₂Cl₂, 15 min, 2.) CH₂Cl₂, 8 h

With 2-isobutoxy-1-isobutoxycarbonyl-1,2-dihydroquinoline; sodium phosphate buffer; lipase A₆ (Amano); triethylamine; In dichloromethane; acetone;
DOI:10.1055/s-1997-1374

Reference yield:

: 4515-24-6
2-acetamido-2-deoxy-3,4,6-tri-O-acetyl-β-D-glucopyranosylamine

: 202266-07-7
N-benzyloxycarbonyl-L-aspartic acid α-(2-methoxyethyl) ester

: 202266-11-3
(S)-2-Benzyloxycarbonylamino-N-((2R,3R,4R,5S,6R)-4,5-diacetoxy-6-acetoxymethyl-3-acetylamino-tetrahydro-pyran-2-yl)-succinamic acid 2-methoxy-ethyl ester

Guidance literature:: With 2-isobutoxy-1-isobutoxycarbonyl-1,2-dihydroquinoline; Yield given. Multistep reaction; 1.) CH₂Cl₂, 15 min, 2.) CH₂Cl₂, 8 h;
DOI:10.1055/s-1997-1374