2-acetamido-3,4,6-tri-O-acetyl-1-N-[α-(carbobenzyloxy)-β-aspartyl]-2-deoxy-β-D-glucopyranosylamine

Base Information

Chemical Name:2-acetamido-3,4,6-tri-O-acetyl-1-N-[α-(carbobenzyloxy)-β-aspartyl]-2-deoxy-β-D-glucopyranosylamine
CAS No.:38877-33-7
Molecular Formula:C₂₆H₃₃N₃O₁₃
Molecular Weight:595.56
Hs Code.:

Synonyms:2-acetamido-3,4,6-tri-O-acetyl-1-N-[α-(carbobenzyloxy)-β-aspartyl]-2-deoxy-β-D-glucopyranosylamine

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Chemical Property of 2-acetamido-3,4,6-tri-O-acetyl-1-N-[α-(carbobenzyloxy)-β-aspartyl]-2-deoxy-β-D-glucopyranosylamine

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Technology Process of 2-acetamido-3,4,6-tri-O-acetyl-1-N-[α-(carbobenzyloxy)-β-aspartyl]-2-deoxy-β-D-glucopyranosylamine

There total 6 articles about 2-acetamido-3,4,6-tri-O-acetyl-1-N-[α-(carbobenzyloxy)-β-aspartyl]-2-deoxy-β-D-glucopyranosylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 202266-11-3
(S)-2-Benzyloxycarbonylamino-N-((2R,3R,4R,5S,6R)-4,5-diacetoxy-6-acetoxymethyl-3-acetylamino-tetrahydro-pyran-2-yl)-succinamic acid 2-methoxy-ethyl ester

: 38877-33-7
2-acetamido-3,4,6-tri-O-acetyl-1-N-[α-(carbobenzyloxy)-β-aspartyl]-2-deoxy-β-D-glucopyranosylamine

Guidance literature:: With sodium phosphate buffer; lipase A₆ (Amano); In acetone; at 37 ℃; for 14h;
DOI:10.1055/s-1997-1374

Reference yield: 70.0%

: 129835-74-1
Z-Asnβ-(Ac3GlcNAc)α-OBu^t

: 38877-33-7
2-acetamido-3,4,6-tri-O-acetyl-1-N-[α-(carbobenzyloxy)-β-aspartyl]-2-deoxy-β-D-glucopyranosylamine

Guidance literature:: With trifluoroacetic acid; In dichloromethane; for 0.5h; Ambient temperature;
DOI:10.1021/jo00313a013

Reference yield:

: 4515-24-6
2-acetamido-2-deoxy-3,4,6-tri-O-acetyl-β-D-glucopyranosylamine

: 38877-33-7
2-acetamido-3,4,6-tri-O-acetyl-1-N-[α-(carbobenzyloxy)-β-aspartyl]-2-deoxy-β-D-glucopyranosylamine

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) isobutyl 2-isobutoxy-1,2-dihydroquinoline-1-carboxylate / 1.) CH₂Cl₂, 15 min, 2.) CH₂Cl₂, 8 h

2: 77 percent / aq. sodium phosphate buffer, lipase A₆ (Amano) / acetone / 14 h / 37 °C

With 2-isobutoxy-1-isobutoxycarbonyl-1,2-dihydroquinoline; sodium phosphate buffer; lipase A₆ (Amano); In acetone;
DOI:10.1055/s-1997-1374