Technology Process of 2-methyl-6-(m-tolyl)phenanthridine
There total 5 articles about 2-methyl-6-(m-tolyl)phenanthridine which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
tert.-butylnitrite; sodium acetate; N,N`-dimethylethylenediamine; dibenzoyl peroxide;
at 20 - 70 ℃;
for 3.08333h;
Schlenk technique;
Inert atmosphere;
DOI:10.1021/ol500923t
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: potassium carbonate / water; 1,2-dimethoxyethane / 0.5 h / 20 °C / Inert atmosphere
1.2: 20 - 80 °C / Inert atmosphere
2.1: tetrahydrofuran / 2 h / 0 - 20 °C
3.1: triethylamine; trichlorophosphate / tetrahydrofuran / 3 h / 0 °C / Inert atmosphere
4.1: dibenzoyl peroxide; sodium acetate; N,N`-dimethylethylenediamine; tert.-butylnitrite / 3.08 h / 20 - 70 °C / Schlenk technique; Inert atmosphere
With
tert.-butylnitrite; sodium acetate; potassium carbonate; triethylamine; N,N`-dimethylethylenediamine; trichlorophosphate; dibenzoyl peroxide;
In
tetrahydrofuran; 1,2-dimethoxyethane; water;
DOI:10.1021/ol500923t
- Guidance literature:
-
Multi-step reaction with 2 steps
1: triethylamine; trichlorophosphate / tetrahydrofuran / 3 h / 0 °C / Inert atmosphere
2: dibenzoyl peroxide; sodium acetate; N,N`-dimethylethylenediamine; tert.-butylnitrite / 3.08 h / 20 - 70 °C / Schlenk technique; Inert atmosphere
With
tert.-butylnitrite; sodium acetate; triethylamine; N,N`-dimethylethylenediamine; trichlorophosphate; dibenzoyl peroxide;
In
tetrahydrofuran;
DOI:10.1021/ol500923t
