N,N-diphenyl-4-(5-cyanopyridin-2-yl)aniline

Base Information

• Chemical Name: N,N-diphenyl-4-(5-cyanopyridin-2-yl)aniline
• CAS No.: 1422183-11-6
• Molecular Formula: C₂₄H₁₇N₃
• Molecular Weight: 347.419
• Mol file: 1422183-11-6.mol

Synonyms:N,N-diphenyl-4-(5-cyanopyridin-2-yl)aniline

Chemical Property of N,N-diphenyl-4-(5-cyanopyridin-2-yl)aniline

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N,N-diphenyl-4-(5-cyanopyridin-2-yl)aniline

There total 1 articles about N,N-diphenyl-4-(5-cyanopyridin-2-yl)aniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

2-bromo-5-cyanopyridine (139585-70-9) + 4-(diphenylamino)phenyl boronic acid (201802-67-7) → N,N-diphenyl-4-(5-cyanopyridin-2-yl)aniline (1422183-11-6)

Guidance literature:

With palladium diacetate; potassium carbonate; In ethanol; water; at 80 ℃; for 0.5h;

DOI:10.1039/c2ra22275b

Reference yield: 40.6%

potassium tetrachloroplatinate(II) (10025-99-7) + N,N-diphenyl-4-(5-cyanopyridin-2-yl)aniline (1422183-11-6) + acetylacetone (123-54-6,81235-32-7) → C29H23N3O2Pt

Guidance literature:

potassium tetrachloroplatinate(II); N,N-diphenyl-4-(5-cyanopyridin-2-yl)aniline; In water; at 100 ℃; for 12h; Inert atmosphere;

acetylacetone; With sodium carbonate; In water; at 100 ℃; for 13h; Inert atmosphere;

Reference yield:

potassium tetrachloroplatinate(II) (10025-99-7) + N,N-diphenyl-4-(5-cyanopyridin-2-yl)aniline (1422183-11-6) → C48H32Cl2N6Pt2 (1496617-71-0)

Guidance literature:

In 2-ethoxy-ethanol; water; at 80 ℃; Inert atmosphere;

DOI:10.1016/j.dyepig.2013.09.030

upstream raw materials:

2-bromo-5-cyanopyridine

4-(diphenylamino)phenyl boronic acid

Downstream raw materials:

C₄₈H₃₂Cl₂N₆Pt₂