3,5-di-tert-butyl-4-hydroxybenzaldehyde dimethyl acetal

Base Information

• Chemical Name: 3,5-di-tert-butyl-4-hydroxybenzaldehyde dimethyl acetal
• CAS No.: 23093-16-5
• Molecular Formula: C₁₇H₂₈O₃
• Molecular Weight: 280.408

Synonyms:3,5-di-tert-butyl-4-hydroxybenzaldehyde dimethyl acetal

Chemical Property of 3,5-di-tert-butyl-4-hydroxybenzaldehyde dimethyl acetal

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

SDS file from LookChem

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Technology Process of 3,5-di-tert-butyl-4-hydroxybenzaldehyde dimethyl acetal

There total 3 articles about 3,5-di-tert-butyl-4-hydroxybenzaldehyde dimethyl acetal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.0%

orthoformic acid triethyl ester (122-51-0) + 3,5-di-t-butyl-4-hydroxybenzaldehyde (1620-98-0) → 3,5-di-tert-butyl-4-hydroxybenzaldehyde dimethyl acetal (23093-16-5)

Guidance literature:

With ammonium chloride; In methanol; for 3.5h; Reflux; Inert atmosphere;

DOI:10.1021/ml500162z

Reference yield:

trimethyl orthoformate (149-73-5) + 3,5-di-t-butyl-4-hydroxybenzaldehyde (1620-98-0) → 3,5-di-tert-butyl-4-hydroxybenzaldehyde dimethyl acetal (23093-16-5)

Guidance literature:

With ammonium chloride; In methanol; xylene; for 2h; Heating;

DOI:10.1021/jo0106795

Reference yield:

→ 3,5-di-tert-butyl-4-hydroxybenzaldehyde dimethyl acetal (23093-16-5)

Guidance literature:

3,5-Di-t-butyl-4-hydroxybenzaldehyd, HC(OMe)3 ;

DOI:10.1021/jo00836a028

upstream raw materials:

trimethyl orthoformate

3,5-di-t-butyl-4-hydroxybenzaldehyde

orthoformic acid triethyl ester

Downstream raw materials:

methyl 3,5-di-tert-butyl-4-hydroxybenzoate

2,6-di-tert-butyl-4-(methoxymethylene)cyclohexa-2,5-dienone

CLH₃₀₄a

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