N(C₂H₅)4⁽¹⁺⁾*W(OC₆H₅)(S₂C₂(C₆H₅)2)2^(1-)=N(C₂H₅)4W(OC₆H₅)(S₂C₂(C₆H₅)2)2

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Chemical Name:N(C₂H₅)4⁽¹⁺⁾*W(OC₆H₅)(S₂C₂(C₆H₅)2)2^(1-)=N(C₂H₅)4W(OC₆H₅)(S₂C₂(C₆H₅)2)2
CAS No.:426209-91-8
Molecular Formula:C₈H₂₀N*C₃₄H₂₅OS₄W
Molecular Weight:891.939
Hs Code.:

N(C<sub>2</sub>H<sub>5</sub>)4<sup>(1+)</sup>*W(OC<sub>6</sub>H<sub>5</sub>)(S<sub>2</sub>C<sub>2</sub>(C<sub>6</sub>H<sub>5</sub>)2)2<sup>(1-)</sup>=N(C<sub>2</sub>H<sub>5</sub>)4W(OC<sub>6</sub>H<sub>5</sub>)(S<sub>2</sub>C<sub>2</sub>(C<sub>6</sub>H<sub>5</sub>)2)2

Synonyms:N(C₂H₅)4⁽¹⁺⁾*W(OC₆H₅)(S₂C₂(C₆H₅)2)2^(1-)=N(C₂H₅)4W(OC₆H₅)(S₂C₂(C₆H₅)2)2

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Chemical Property of N(C₂H₅)4⁽¹⁺⁾*W(OC₆H₅)(S₂C₂(C₆H₅)2)2^(1-)=N(C₂H₅)4W(OC₆H₅)(S₂C₂(C₆H₅)2)2

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Technology Process of N(C₂H₅)4⁽¹⁺⁾*W(OC₆H₅)(S₂C₂(C₆H₅)2)2^(1-)=N(C₂H₅)4W(OC₆H₅)(S₂C₂(C₆H₅)2)2

There total 1 articles about N(C₂H₅)4⁽¹⁺⁾*W(OC₆H₅)(S₂C₂(C₆H₅)2)2^(1-)=N(C₂H₅)4W(OC₆H₅)(S₂C₂(C₆H₅)2)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 34.0%

: 12123-74-9,25282-61-5
W(S₂C₂Ph₂)₂(CO)₂

: 56-34-8
tetraethylammonium chloride

: 139-02-6
sodium phenoxide

: 426209-91-8
N(C₂H₅)4⁽¹⁺⁾*W(OC₆H₅)(S₂C₂(C₆H₅)2)2^(1-)=N(C₂H₅)4W(OC₆H₅)(S₂C₂(C₆H₅)2)2

Guidance literature:: In tetrahydrofuran; acetonitrile; byproducts: CO, NaCl; to a soln. of complex in THF was added a solid NaOPh, stirred for 1 h, treated with Et4NCl in acetonitrile (N2); the solvents were removed, the solid was dissolved in acetonitrile and filtered, ether was layered on the filtrate over 1 d, the solid was washed with ether and dried; elem. anal.;
DOI:10.1021/ja0036559

Reference yield:

: 426209-91-8
N(C₂H₅)4⁽¹⁺⁾*W(OC₆H₅)(S₂C₂(C₆H₅)2)2^(1-)=N(C₂H₅)4W(OC₆H₅)(S₂C₂(C₆H₅)2)2

: N(C₂H₅)4⁽¹⁺⁾*WO(OC₆H₅)(S₂C₂(C₆H₅)2)2^(1-)=N(C₂H₅)4WO(OC₆H₅)(S₂C₂(C₆H₅)2)2

Guidance literature:: With (CH₃)3NO; In acetonitrile; to a frozen soln. of complex in CH3CN was injected a soln. of Me3NO in CH3CN, warmed to -15°C over 30 min (N2); detected by UV spectra;
DOI:10.1021/ja0036559