1-[4,6-di-O-(tert-butyldimethylsilyl)-2,3-dideoxy-β-D-erythro-hex-2-enopyranosyl]-4-n-propylbenzene

Base Information

Chemical Name:1-[4,6-di-O-(tert-butyldimethylsilyl)-2,3-dideoxy-β-D-erythro-hex-2-enopyranosyl]-4-n-propylbenzene
CAS No.:404872-00-0
Molecular Formula:C₂₇H₄₈O₃Si₂
Molecular Weight:476.847
Hs Code.:

Synonyms:1-[4,6-di-O-(tert-butyldimethylsilyl)-2,3-dideoxy-β-D-erythro-hex-2-enopyranosyl]-4-n-propylbenzene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-[4,6-di-O-(tert-butyldimethylsilyl)-2,3-dideoxy-β-D-erythro-hex-2-enopyranosyl]-4-n-propylbenzene

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Technology Process of 1-[4,6-di-O-(tert-butyldimethylsilyl)-2,3-dideoxy-β-D-erythro-hex-2-enopyranosyl]-4-n-propylbenzene

There total 1 articles about 1-[4,6-di-O-(tert-butyldimethylsilyl)-2,3-dideoxy-β-D-erythro-hex-2-enopyranosyl]-4-n-propylbenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 87942-08-3
bromo(4-propylphenyl)magnesium

: 201232-73-7
p-tert-butylphenyl 4,6-di-O-tert-butyl(dimethyl)silyl-2,3-dideoxy-α-D-erythro-hex-2-enopyranoside

: 404872-00-0
1-[4,6-di-O-(tert-butyldimethylsilyl)-2,3-dideoxy-β-D-erythro-hex-2-enopyranosyl]-4-n-propylbenzene

Guidance literature:: With 1,2-bis(diphenylphosphino)ethane nickel(II) chloride; In tetrahydrofuran; at -40 ℃; for 24h;

Reference yield: 80.0%

: 404872-00-0
1-[4,6-di-O-(tert-butyldimethylsilyl)-2,3-dideoxy-β-D-erythro-hex-2-enopyranosyl]-4-n-propylbenzene

: 404872-06-6
1-(2,3-dideoxy-β-D-erythro-hex-2-enopyranosyl)-4-n-propylbenzene

Guidance literature:: With tetrabutyl-ammonium chloride; In tetrahydrofuran; at 25 ℃; for 2h;

Reference yield:

: 404872-00-0
1-[4,6-di-O-(tert-butyldimethylsilyl)-2,3-dideoxy-β-D-erythro-hex-2-enopyranosyl]-4-n-propylbenzene

: 404872-12-4
1-(2,3-dideoxy-β-D-erythro-hexanopyranosyl)-4-n-propylbenzene

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / tetrabutylammonium chloride trihydrate / tetrahydrofuran / 2 h / 25 °C

2: 86 percent / H₂ / [Rh(COD)(1,4-bis(diphenylphosphino)butane)]ClO₄ / ethanol / 24 h / 20 °C / atmospheric pressure

With tetrabutyl-ammonium chloride; hydrogen; [Rh(COD)(1,4-bis(diphenylphosphino)butane)]ClO₄; In tetrahydrofuran; ethanol;