6-O-benzyl-5a-carba-N-dodecanoyl-3,4-O-isopropylidene-N-octadecyl-β-D-galactopyranosylamine

Base Information

Chemical Name:6-O-benzyl-5a-carba-N-dodecanoyl-3,4-O-isopropylidene-N-octadecyl-β-D-galactopyranosylamine
CAS No.:157609-14-8
Molecular Formula:C₄₇H₈₃NO₅
Molecular Weight:742.18
Hs Code.:

Synonyms:6-O-benzyl-5a-carba-N-dodecanoyl-3,4-O-isopropylidene-N-octadecyl-β-D-galactopyranosylamine

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Chemical Property of 6-O-benzyl-5a-carba-N-dodecanoyl-3,4-O-isopropylidene-N-octadecyl-β-D-galactopyranosylamine

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Technology Process of 6-O-benzyl-5a-carba-N-dodecanoyl-3,4-O-isopropylidene-N-octadecyl-β-D-galactopyranosylamine

There total 8 articles about 6-O-benzyl-5a-carba-N-dodecanoyl-3,4-O-isopropylidene-N-octadecyl-β-D-galactopyranosylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: 143-07-7
lauric acid

: 157609-13-7
6-O-benzyl-5a-carba-3,4-O-isopropylidene-N-octadecyl-β-D-galactopyranosylamine

: 157609-14-8
6-O-benzyl-5a-carba-N-dodecanoyl-3,4-O-isopropylidene-N-octadecyl-β-D-galactopyranosylamine

Guidance literature:: With diethyl cyanophosphonate; triethylamine; In N,N-dimethyl-formamide; at 0 ℃; for 3h;

Reference yield:

: 143058-81-5
(1R)-(1,3/2)-3-hydroxymethyl-5-cyclohexene-1,2-diol

: 157609-14-8
6-O-benzyl-5a-carba-N-dodecanoyl-3,4-O-isopropylidene-N-octadecyl-β-D-galactopyranosylamine

Guidance literature:: Multi-step reaction with 9 steps

1: 82 percent / pyridine / 1.) -15 deg C, 1 h, 2.) r.t., 3 h

2: 100 percent / pyridine / 3 h / 0 °C

3: dimethylformamide; H₂O / 18 h / 120 °C

4: 0.1M CH₃ONa / methanol / 2 h / Ambient temperature

5: p-TsOH*H₂O / dimethylformamide / 1 h / Ambient temperature

6: 94 percent / NaH / dimethylformamide / 0.5 h / Ambient temperature

7: 99 percent / m-chloroperbenzoic acid, 1M Na₂HPO₄, 1M NaH₂PO₄ / H₂O / 3 h / Ambient temperature

8: 78 percent / propan-2-ol / 96 h / 120 °C

9: 57 percent / diethyl cyanophosphonate, Et₃N / dimethylformamide / 3 h / 0 °C

With pyridine; disodium hydrogenphosphate; sodium dihydrogenphosphate; diethyl cyanophosphonate; sodium methylate; sodium hydride; toluene-4-sulfonic acid; triethylamine; 3-chloro-benzenecarboperoxoic acid; In methanol; water; N,N-dimethyl-formamide; isopropyl alcohol;

Reference yield:

: 157609-10-4
(1S,2R,6R)-2-hydroxymethyl-8,8-dimethyl-7,9-dioxabicyclo<4.3.0>non-4-ene

: 157609-14-8
6-O-benzyl-5a-carba-N-dodecanoyl-3,4-O-isopropylidene-N-octadecyl-β-D-galactopyranosylamine

Guidance literature:: Multi-step reaction with 4 steps

1: 94 percent / NaH / dimethylformamide / 0.5 h / Ambient temperature

2: 99 percent / m-chloroperbenzoic acid, 1M Na₂HPO₄, 1M NaH₂PO₄ / H₂O / 3 h / Ambient temperature

3: 78 percent / propan-2-ol / 96 h / 120 °C

4: 57 percent / diethyl cyanophosphonate, Et₃N / dimethylformamide / 3 h / 0 °C

With disodium hydrogenphosphate; sodium dihydrogenphosphate; diethyl cyanophosphonate; sodium hydride; triethylamine; 3-chloro-benzenecarboperoxoic acid; In water; N,N-dimethyl-formamide; isopropyl alcohol;