monotritylated bis-N,N'-(2-(2-(2-(2-hydroxyethoxy)ethoxy)ethoxy)ethyl) perylenetetracarboxylic diimide

Base Information

• Chemical Name: monotritylated bis-N,N'-(2-(2-(2-(2-hydroxyethoxy)ethoxy)ethoxy)ethyl) perylenetetracarboxylic diimide
• CAS No.: 791074-68-5
• Molecular Formula: C₆₁H₆₀N₂O₁₄
• Molecular Weight: 1045.15

Synonyms:monotritylated bis-N,N'-(2-(2-(2-(2-hydroxyethoxy)ethoxy)ethoxy)ethyl) perylenetetracarboxylic diimide

Chemical Property of monotritylated bis-N,N'-(2-(2-(2-(2-hydroxyethoxy)ethoxy)ethoxy)ethyl) perylenetetracarboxylic diimide

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Technology Process of monotritylated bis-N,N'-(2-(2-(2-(2-hydroxyethoxy)ethoxy)ethoxy)ethyl) perylenetetracarboxylic diimide

There total 3 articles about monotritylated bis-N,N'-(2-(2-(2-(2-hydroxyethoxy)ethoxy)ethoxy)ethyl) perylenetetracarboxylic diimide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.0%

bis-N,N’-(2-(2-(2-(2-thioacetylethoxy)ethoxy)ethoxy)ethyl)-3,4,9,10-perylene tetracarboxylic diimide (500883-28-3) + 4,4'-dimethoxytrityl chloride (40615-36-9) → monotritylated bis-N,N'-(2-(2-(2-(2-hydroxyethoxy)ethoxy)ethoxy)ethyl) perylenetetracarboxylic diimide (791074-68-5) + 2,9-bis-{2-[2-(2-{2-[bis-(4-methoxy-phenyl)-phenyl-methoxy]-ethoxy}-ethoxy)-ethoxy]-ethyl}-anthra[2,1,9-def;6,5,10-d'e'f']diisoquinoline-1,3,8,10-tetraone

Guidance literature:

With pyridine; dmap; at 20 ℃;

DOI:10.1021/ja027186h

Reference yield: 17.6%

2,9-bis-{2-[2-(2-{2-[bis-(4-methoxy-phenyl)-phenyl-methoxy]-ethoxy}-ethoxy)-ethoxy]-ethyl}-anthra[2,1,9-def;6,5,10-d'e'f']diisoquinoline-1,3,8,10-tetraone → bis-N,N’-(2-(2-(2-(2-thioacetylethoxy)ethoxy)ethoxy)ethyl)-3,4,9,10-perylene tetracarboxylic diimide (500883-28-3) + monotritylated bis-N,N'-(2-(2-(2-(2-hydroxyethoxy)ethoxy)ethoxy)ethyl) perylenetetracarboxylic diimide (791074-68-5)

Guidance literature:

With methanol; zinc(II) chloride; In dichloromethane; Product distribution / selectivity;

Reference yield:

2,9-bis-{2-[2-(2-{2-[bis-(4-methoxy-phenyl)-phenyl-methoxy]-ethoxy}-ethoxy)-ethoxy]-ethyl}-anthra[2,1,9-def;6,5,10-d'e'f']diisoquinoline-1,3,8,10-tetraone → monotritylated bis-N,N'-(2-(2-(2-(2-hydroxyethoxy)ethoxy)ethoxy)ethyl) perylenetetracarboxylic diimide (791074-68-5)

Guidance literature:

With zinc(II) chloride; In methanol; dichloromethane;

DOI:10.1021/ja027186h

upstream raw materials:

bis-N,N’-(2-(2-(2-(2-thioacetylethoxy)ethoxy)ethoxy)ethyl)-3,4,9,10-perylene tetracarboxylic diimide

4,4'-dimethoxytrityl chloride

Downstream raw materials:

C₇₀H₇₇N₄O₁₅P

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