bis-N,N’-(2-(2-(2-(2-thioacetylethoxy)ethoxy)ethoxy)ethyl)-3,4,9,10-perylene tetracarboxylic diimide

Base Information

• Chemical Name: bis-N,N’-(2-(2-(2-(2-thioacetylethoxy)ethoxy)ethoxy)ethyl)-3,4,9,10-perylene tetracarboxylic diimide
• CAS No.: 500883-28-3
• Molecular Formula: C₄₀H₄₂N₂O₁₂
• Molecular Weight: 742.78

Synonyms:bis-N,N’-(2-(2-(2-(2-thioacetylethoxy)ethoxy)ethoxy)ethyl)-3,4,9,10-perylene tetracarboxylic diimide

Chemical Property of bis-N,N’-(2-(2-(2-(2-thioacetylethoxy)ethoxy)ethoxy)ethyl)-3,4,9,10-perylene tetracarboxylic diimide

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Technology Process of bis-N,N’-(2-(2-(2-(2-thioacetylethoxy)ethoxy)ethoxy)ethyl)-3,4,9,10-perylene tetracarboxylic diimide

There total 1 articles about bis-N,N’-(2-(2-(2-(2-thioacetylethoxy)ethoxy)ethoxy)ethyl)-3,4,9,10-perylene tetracarboxylic diimide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 17.6%

2,9-bis-{2-[2-(2-{2-[bis-(4-methoxy-phenyl)-phenyl-methoxy]-ethoxy}-ethoxy)-ethoxy]-ethyl}-anthra[2,1,9-def;6,5,10-d'e'f']diisoquinoline-1,3,8,10-tetraone → bis-N,N’-(2-(2-(2-(2-thioacetylethoxy)ethoxy)ethoxy)ethyl)-3,4,9,10-perylene tetracarboxylic diimide (500883-28-3) + monotritylated bis-N,N'-(2-(2-(2-(2-hydroxyethoxy)ethoxy)ethoxy)ethyl) perylenetetracarboxylic diimide (791074-68-5)

Guidance literature:

With methanol; zinc(II) chloride; In dichloromethane; Product distribution / selectivity;

Reference yield: 30.0%

bis-N,N’-(2-(2-(2-(2-thioacetylethoxy)ethoxy)ethoxy)ethyl)-3,4,9,10-perylene tetracarboxylic diimide (500883-28-3) + 4,4'-dimethoxytrityl chloride (40615-36-9) → monotritylated bis-N,N'-(2-(2-(2-(2-hydroxyethoxy)ethoxy)ethoxy)ethyl) perylenetetracarboxylic diimide (791074-68-5) + 2,9-bis-{2-[2-(2-{2-[bis-(4-methoxy-phenyl)-phenyl-methoxy]-ethoxy}-ethoxy)-ethoxy]-ethyl}-anthra[2,1,9-def;6,5,10-d'e'f']diisoquinoline-1,3,8,10-tetraone

Guidance literature:

With pyridine; dmap; at 20 ℃;

DOI:10.1021/ja027186h

Reference yield: 22.5%

bis-N,N’-(2-(2-(2-(2-thioacetylethoxy)ethoxy)ethoxy)ethyl)-3,4,9,10-perylene tetracarboxylic diimide (500883-28-3) + benzoyl chloride (98-88-4) → C54H50N2O14 + benzoic acid 2-[2-(2-{2-[9-(2-{2-[2-(2-hydroxy-ethoxy)-ethoxy]-ethoxy}-ethyl)-1,3,8,10-tetraoxo-3,8,9,10-tetrahydro-1H-anthra[2,1,9-def;6,5,10-d'e'f']diisoquinolin-2-yl]-ethoxy}-ethoxy)-ethoxy]-ethyl ester

Guidance literature:

With pyridine; dmap; at 20 ℃;

DOI:10.1021/ja027186h

Downstream raw materials:

monotritylated bis-N,N'-(2-(2-(2-(2-hydroxyethoxy)ethoxy)ethoxy)ethyl) perylenetetracarboxylic diimide

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