1-[2-(1,3-dimethylxanthin-7-yl)acetyl]-4-(4-chlorophenyl)thiosemicarbazide

Base Information

Chemical Name:1-[2-(1,3-dimethylxanthin-7-yl)acetyl]-4-(4-chlorophenyl)thiosemicarbazide
CAS No.:145746-87-8
Molecular Formula:C₁₆H₁₆ClN₇O₃S
Molecular Weight:421.867
Hs Code.:

Synonyms:1-[2-(1,3-dimethylxanthin-7-yl)acetyl]-4-(4-chlorophenyl)thiosemicarbazide

Suppliers and Price of 1-[2-(1,3-dimethylxanthin-7-yl)acetyl]-4-(4-chlorophenyl)thiosemicarbazide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 1-[2-(1,3-dimethylxanthin-7-yl)acetyl]-4-(4-chlorophenyl)thiosemicarbazide

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 1-[2-(1,3-dimethylxanthin-7-yl)acetyl]-4-(4-chlorophenyl)thiosemicarbazide

There total 2 articles about 1-[2-(1,3-dimethylxanthin-7-yl)acetyl]-4-(4-chlorophenyl)thiosemicarbazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 41838-25-9
2-(1,3-dimethyl-2,6-dioxo-1,2,3,6-tetrahydro-7H-purin-7-yl)acetohydrazide

: 2131-55-7
4-Chlorophenyl isothiocyanate

: 145746-87-8
1-[2-(1,3-dimethylxanthin-7-yl)acetyl]-4-(4-chlorophenyl)thiosemicarbazide

Guidance literature:: In 1,3-dioxane; for 6h; Reflux;
DOI:10.3390/molecules18089684

Reference yield:

: 58-55-9,75448-53-2
theophylline

: 145746-87-8
1-[2-(1,3-dimethylxanthin-7-yl)acetyl]-4-(4-chlorophenyl)thiosemicarbazide

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium; methanol

1.2: 7 h / Heating

2.1: hydrazine hydrate / ethanol / 6 h / Heating

3.1: 1,3-dioxane / 6 h / Reflux

With methanol; sodium; hydrazine hydrate; In 1,3-dioxane; ethanol;
DOI:10.3390/molecules18089684