3,4-Diiodobenzotrifluoride

Base Information

Chemical Name:3,4-Diiodobenzotrifluoride
CAS No.:130656-70-1
Molecular Formula:C₇H₃F₃I₂
Molecular Weight:397.905
Hs Code.:
DSSTox Substance ID:DTXSID20443899
Wikidata:Q82261883
Mol file:130656-70-1.mol

Synonyms:3,4-Diiodobenzotrifluoride;130656-70-1;1,2-diiodo-4-(trifluoromethyl)benzene;SCHEMBL7863217;DTXSID20443899;VJVPAKPVOCXMDE-UHFFFAOYSA-N

Suppliers and Price of 3,4-Diiodobenzotrifluoride

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
3,4-DIIODOBENZOTRIFLUORIDE 95.00%
5MG
$ 504.56

AHH
3,4-Diiodobenzotrifluoride 98%
25g
$ 680.00

Total 7 raw suppliers

Chemical Property of 3,4-Diiodobenzotrifluoride

Chemical Property:

XLogP3:4.1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:0
Exact Mass:397.82763
Heavy Atom Count:12
Complexity:157

Purity/Quality:

98%min ^*data from raw suppliers

3,4-DIIODOBENZOTRIFLUORIDE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC(=C(C=C1C(F)(F)F)I)I

Technology Process of 3,4-Diiodobenzotrifluoride

There total 2 articles about 3,4-Diiodobenzotrifluoride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 163444-17-5
2-iodo-4-(trifluoromethyl)aniline

: 130656-70-1
1,2-diiodo-4-trifluoromethylbenzene

Guidance literature:: 2-iodo-4-(trifluoromethyl)aniline; With hydrogenchloride; sodium nitrite; In water; at -11 - -9 ℃; for 1h;

With sulfuric acid; potassium iodide; In water; at 0 - 53 ℃;

Reference yield:

: 455-14-1
4-trifluoromethylphenylamine

: 130656-70-1
1,2-diiodo-4-trifluoromethylbenzene

Guidance literature:: Multi-step reaction with 2 steps

1.1: 546 g / benzyltrimethylammonium dichloroiodide; CaCO₃ / CH₂Cl₂; methanol / 30 h

2.1: NaNO₂; HCl / H₂O / 1 h / -11 - -9 °C

2.2: 256 g / H₂SO₄; KI / H₂O / 0 - 53 °C

With hydrogenchloride; N,N,N-trimethylbenzenemethanaminium dichloroiodate; calcium carbonate; sodium nitrite; In methanol; dichloromethane; water; 2.1: Griess diazotisation / 2.2: Sandmeyer substitution;

Reference yield: 75.0%

: 292638-85-8,9003-21-8,96-33-3
acrylic acid methyl ester

: 6163-58-2
tris-(o-tolyl)phosphine

: 130656-70-1
1,2-diiodo-4-trifluoromethylbenzene

: 4-trifluoromethyl-1,2-di-(β-methoxycarbonylvinyl)-benzene

Guidance literature:: With triethylamine; palladium diacetate; In 5,5-dimethyl-1,3-cyclohexadiene; diethyl ether; cyclohexane; Petroleum ether;