C₁₆H₁₇NO₂S

Base Information

Chemical Name:C₁₆H₁₇NO₂S
CAS No.:1448354-54-8
Molecular Formula:C₁₆H₁₇NO₂S
Molecular Weight:287.382
Hs Code.:

C<sub>16</sub>H<sub>17</sub>NO<sub>2</sub>S

Synonyms:C₁₆H₁₇NO₂S

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Chemical Property of C₁₆H₁₇NO₂S

Chemical Property:

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Technology Process of C₁₆H₁₇NO₂S

There total 3 articles about C₁₆H₁₇NO₂S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 3262-89-3
triphenylboroxine

: 16851-71-1
1-(benzenesulfonyl)-2,5-dihydro-1H-pyrrole

: 1448354-54-8
C₁₆H₁₇NO₂S

Guidance literature:: With [Rh(OH)(coe)₂]₂; (R)-segphos; In tetrahydrofuran; water; at 23 ℃; for 24h; enantioselective reaction; Inert atmosphere;
DOI:10.1021/ja406169s

Reference yield:

: 25630-24-4
N,N-diallylbenzenesulfonamide

: 1448354-54-8
C₁₆H₁₇NO₂S

Guidance literature:: Multi-step reaction with 2 steps

1: Grubbs catalyst first generation / dichloromethane / 20 °C / Inert atmosphere

2: [Rh(OH)(coe)₂]₂; (R)-segphos / tetrahydrofuran; water / 24 h / 23 °C / Inert atmosphere

With Grubbs catalyst first generation; [Rh(OH)(coe)₂]₂; (R)-segphos; In tetrahydrofuran; dichloromethane; water;
DOI:10.1021/ja406169s

Reference yield:

: 98-09-9
benzenesulfonyl chloride

: 1448354-54-8
C₁₆H₁₇NO₂S

Guidance literature:: Multi-step reaction with 3 steps

1.1: triethylamine / dichloromethane / 0 °C / Inert atmosphere

1.2: 0 - 20 °C / Inert atmosphere

2.1: Grubbs catalyst first generation / dichloromethane / 20 °C / Inert atmosphere

3.1: [Rh(OH)(coe)₂]₂; (R)-segphos / tetrahydrofuran; water / 24 h / 23 °C / Inert atmosphere

With Grubbs catalyst first generation; [Rh(OH)(coe)₂]₂; triethylamine; (R)-segphos; In tetrahydrofuran; dichloromethane; water;
DOI:10.1021/ja406169s