α-(di-t-butylphosphino)-α'-{bis(pentafluorophenyl)phosphino}-o-xylene-borane

Base Information

Chemical Name:α-(di-t-butylphosphino)-α'-{bis(pentafluorophenyl)phosphino}-o-xylene-borane
CAS No.:1543108-64-0
Molecular Formula:C₂₈H₂₉BF₁₀P₂
Molecular Weight:628.281
Hs Code.:

Synonyms:α-(di-t-butylphosphino)-α'-{bis(pentafluorophenyl)phosphino}-o-xylene-borane

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Chemical Property of α-(di-t-butylphosphino)-α'-{bis(pentafluorophenyl)phosphino}-o-xylene-borane

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Technology Process of α-(di-t-butylphosphino)-α'-{bis(pentafluorophenyl)phosphino}-o-xylene-borane

There total 1 articles about α-(di-t-butylphosphino)-α'-{bis(pentafluorophenyl)phosphino}-o-xylene-borane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 32.0%

: 1126193-17-6
α-(di-t-butylphosphino)-α'-chloro-o-xylene-borane

: 13648-79-8
bis(pentafluorophenyl)bromophosphine

: 1543108-64-0
α-(di-t-butylphosphino)-α'-{bis(pentafluorophenyl)phosphino}-o-xylene-borane

Guidance literature:: α-(di-t-butylphosphino)-α'-chloro-o-xylene-borane; With magnesium; In tetrahydrofuran; for 2h; Inert atmosphere; Schlenk technique;

bis(pentafluorophenyl)bromophosphine; In tetrahydrofuran; at 0 - 20 ℃; Inert atmosphere; Schlenk technique;
DOI:10.1039/c3ob42244e

Reference yield: 84.0%

: 110-91-8,99108-56-2
morpholine

: 1543108-64-0
α-(di-t-butylphosphino)-α'-{bis(pentafluorophenyl)phosphino}-o-xylene-borane

: 1543108-68-4
α-(di-t-butylphosphino)-α'-{bis(p-N-morpholinotetrafluorophenyl)phosphino}-o-xylene

Guidance literature:: at 100 ℃; for 1h; Inert atmosphere; Sealed tube;
DOI:10.1039/c3ob42244e

Reference yield: 51.0%

: 1543108-64-0
α-(di-t-butylphosphino)-α'-{bis(pentafluorophenyl)phosphino}-o-xylene-borane

: 1543108-67-3
α-(di-t-butylphosphino)-α'-{bis(pentafluorophenyl)phosphino}-o-xylene

Guidance literature:: α-(di-t-butylphosphino)-α'-{bis(pentafluorophenyl)phosphino}-o-xylene-borane; With tetrafluoroboric acid diethyl ether complex; In dichloromethane; at -10 - 20 ℃; for 1h; Inert atmosphere; Schlenk technique;

With sodium hydrogencarbonate; In diethyl ether; dichloromethane; at 20 ℃; for 0.5h; Inert atmosphere; Schlenk technique;
DOI:10.1039/c3ob42244e