N-(methoxycarbonyl)-N-[2-(3,4-methylenedioxyphenyl)-2-cyclohexen-1-yl]trichloroacetamide

Base Information

Chemical Name:N-(methoxycarbonyl)-N-[2-(3,4-methylenedioxyphenyl)-2-cyclohexen-1-yl]trichloroacetamide
CAS No.:256506-17-9
Molecular Formula:C₁₇H₁₆Cl₃NO₅
Molecular Weight:420.677
Hs Code.:

Synonyms:N-(methoxycarbonyl)-N-[2-(3,4-methylenedioxyphenyl)-2-cyclohexen-1-yl]trichloroacetamide

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Chemical Property of N-(methoxycarbonyl)-N-[2-(3,4-methylenedioxyphenyl)-2-cyclohexen-1-yl]trichloroacetamide

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Technology Process of N-(methoxycarbonyl)-N-[2-(3,4-methylenedioxyphenyl)-2-cyclohexen-1-yl]trichloroacetamide

There total 1 articles about N-(methoxycarbonyl)-N-[2-(3,4-methylenedioxyphenyl)-2-cyclohexen-1-yl]trichloroacetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 161196-44-7
methyl 2-(3',4'-methylenedioxyphenyl)cyclohex-2-enylcarbamate

: 76-02-8
trifluoroacetyl chloride

: 256506-17-9
N-(methoxycarbonyl)-N-[2-(3,4-methylenedioxyphenyl)-2-cyclohexen-1-yl]trichloroacetamide

Guidance literature:: methyl 2-(3',4'-methylenedioxyphenyl)cyclohex-2-enylcarbamate; With [2,2]bipyridinyl; n-butyllithium; In tetrahydrofuran; hexane; at -45 - 0 ℃;

trifluoroacetyl chloride; In tetrahydrofuran; hexane; at 20 ℃; for 1h;
DOI:10.1021/jo9912146