O,O-dimethyl (S)-{[(1S)-2-hydroxy-1-phenylethyl]amino}(phenyl)methylphosphonothioate

Base Information

Chemical Name:O,O-dimethyl (S)-{[(1S)-2-hydroxy-1-phenylethyl]amino}(phenyl)methylphosphonothioate
CAS No.:681035-67-6
Molecular Formula:C₁₇H₂₂NO₃PS
Molecular Weight:351.406
Hs Code.:

Synonyms:O,O-dimethyl (S)-{[(1S)-2-hydroxy-1-phenylethyl]amino}(phenyl)methylphosphonothioate

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Chemical Property of O,O-dimethyl (S)-{[(1S)-2-hydroxy-1-phenylethyl]amino}(phenyl)methylphosphonothioate

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Technology Process of O,O-dimethyl (S)-{[(1S)-2-hydroxy-1-phenylethyl]amino}(phenyl)methylphosphonothioate

There total 3 articles about O,O-dimethyl (S)-{[(1S)-2-hydroxy-1-phenylethyl]amino}(phenyl)methylphosphonothioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 44.9%

: 5930-72-3
dimethyl thiophosphite

: 74879-43-9
(S)-2-Phenyl-2-{[1-phenyl-meth-(E)-ylidene]-amino}-ethanol

: 681035-67-6
O,O-dimethyl (S)-{[(1S)-2-hydroxy-1-phenylethyl]amino}(phenyl)methylphosphonothioate

: O,O-dimethyl (R)-{[(1S)-2-hydroxy-1-phenylethyl]amino}(phenyl)methylphosphonothioate

Guidance literature:: In toluene; at 0 ℃; for 12h;
DOI:10.1021/jo035707t

Reference yield:

: 20989-17-7
(2S)-2-phenylglycinol

: 681035-67-6
O,O-dimethyl (S)-{[(1S)-2-hydroxy-1-phenylethyl]amino}(phenyl)methylphosphonothioate

Guidance literature:: Multi-step reaction with 2 steps

1: molecular sieves (3 Angstroem) / toluene / 2 h / 20 °C

2: 6.2 percent / toluene / 12 h / 0 °C

With 3 A molecular sieve; In toluene;
DOI:10.1021/jo035707t

Reference yield:

: 100-52-7
benzaldehyde

: 681035-67-6
O,O-dimethyl (S)-{[(1S)-2-hydroxy-1-phenylethyl]amino}(phenyl)methylphosphonothioate

Guidance literature:: Multi-step reaction with 2 steps

1: molecular sieves (3 Angstroem) / toluene / 2 h / 20 °C

2: 6.2 percent / toluene / 12 h / 0 °C

With 3 A molecular sieve; In toluene;
DOI:10.1021/jo035707t