S-(5,5-dimethyl-3-dimethylamino-2-cyclohexen-1-yliden)-N-(p-methoxyphenylsulfonyl)sulfimid

Base Information

Chemical Name:S-(5,5-dimethyl-3-dimethylamino-2-cyclohexen-1-yliden)-N-(p-methoxyphenylsulfonyl)sulfimid
CAS No.:180038-88-4
Molecular Formula:C₁₇H₂₄N₂O₃S₂
Molecular Weight:368.521
Hs Code.:

Synonyms:S-(5,5-dimethyl-3-dimethylamino-2-cyclohexen-1-yliden)-N-(p-methoxyphenylsulfonyl)sulfimid

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of S-(5,5-dimethyl-3-dimethylamino-2-cyclohexen-1-yliden)-N-(p-methoxyphenylsulfonyl)sulfimid

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Technology Process of S-(5,5-dimethyl-3-dimethylamino-2-cyclohexen-1-yliden)-N-(p-methoxyphenylsulfonyl)sulfimid

There total 2 articles about S-(5,5-dimethyl-3-dimethylamino-2-cyclohexen-1-yliden)-N-(p-methoxyphenylsulfonyl)sulfimid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 57966-11-7
3-N,N-dimethylamino-5,5-dimethyl-2-cyclohexene-1-thione

: 29917-03-1
N-chloro-p-methoxybenzenesulfonamide sodium salt

: 180038-88-4
S-(5,5-dimethyl-3-dimethylamino-2-cyclohexen-1-yliden)-N-(p-methoxyphenylsulfonyl)sulfimid

Guidance literature:: With tetrabutyl-ammonium chloride; In dichloromethane; water; at 0 - 5 ℃; for 0.666667h;
DOI:10.1080/10426509608046351

Reference yield:

: 31039-88-0
3-(dimethylamino)-5,5-dimethyl-2-cyclohexen-1-one

: 180038-88-4
S-(5,5-dimethyl-3-dimethylamino-2-cyclohexen-1-yliden)-N-(p-methoxyphenylsulfonyl)sulfimid

Guidance literature:: Multi-step reaction with 2 steps

1: 64 percent / 2,4-bis(4-methoxyphenyl)-1,3-dithia-2,4-diphosphetane-2,4-disulfide / 1,2-dimethoxy-ethane

2: 65 percent / tetrabutylammonium chloride / CH₂Cl₂; H₂O / 0.67 h / 0 - 5 °C

With Lawessons reagent; tetrabutyl-ammonium chloride; In 1,2-dimethoxyethane; dichloromethane; water;
DOI:10.1080/10426509608046351