isopropyl 7-[[(1'S)-1'-phenylethyl]amino]-6,7-dideoxy-1,2:3,4-di-O-isopropylidene-D-glycero-α-D-galactooctopyranuronate

Base Information

Chemical Name:isopropyl 7-[[(1'S)-1'-phenylethyl]amino]-6,7-dideoxy-1,2:3,4-di-O-isopropylidene-D-glycero-α-D-galactooctopyranuronate
CAS No.:206127-71-1
Molecular Formula:C₂₅H₃₇NO₇
Molecular Weight:463.571
Hs Code.:

Synonyms:isopropyl 7-[[(1'S)-1'-phenylethyl]amino]-6,7-dideoxy-1,2:3,4-di-O-isopropylidene-D-glycero-α-D-galactooctopyranuronate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of isopropyl 7-[[(1'S)-1'-phenylethyl]amino]-6,7-dideoxy-1,2:3,4-di-O-isopropylidene-D-glycero-α-D-galactooctopyranuronate

Chemical Property:

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Technology Process of isopropyl 7-[[(1'S)-1'-phenylethyl]amino]-6,7-dideoxy-1,2:3,4-di-O-isopropylidene-D-glycero-α-D-galactooctopyranuronate

There total 8 articles about isopropyl 7-[[(1'S)-1'-phenylethyl]amino]-6,7-dideoxy-1,2:3,4-di-O-isopropylidene-D-glycero-α-D-galactooctopyranuronate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2-[(E)-(S)-1-Phenyl-ethylimino]-3-((3aR,5R,5aS,8aS,8bR)-2,2,7,7-tetramethyl-tetrahydro-bis[1,3]dioxolo[4,5-b;4',5'-d]pyran-5-yl)-propionic acid isopropyl ester

: 206127-70-0
isopropyl 7-[[(1'S)-1'-phenylethyl]amino]-6,7-dideoxy-1,2:3,4-di-O-isopropylidene-L-glycero-α-D-galactooctopyranuronate

: 206127-71-1
isopropyl 7-[[(1'S)-1'-phenylethyl]amino]-6,7-dideoxy-1,2:3,4-di-O-isopropylidene-D-glycero-α-D-galactooctopyranuronate

Guidance literature:: With hydrogen; palladium on activated charcoal; In isopropyl alcohol; for 8h; under 7500.6 Torr; Yield given. Yields of byproduct given;
DOI:10.1055/s-1998-1660

Reference yield:

: 120449-66-3
isopropyl 6-deoxy-7-oxo-1,2:3,4-di-O-isopropylidene-α-D-galacto-octopyranuronate

: 206127-71-1
isopropyl 7-[[(1'S)-1'-phenylethyl]amino]-6,7-dideoxy-1,2:3,4-di-O-isopropylidene-D-glycero-α-D-galactooctopyranuronate

Guidance literature:: Multi-step reaction with 2 steps

1: benzene / 13 h / Heating

2: H₂ / Pd/C / benzene / 8 h / 20 °C / 7500.6 Torr

With hydrogen; palladium on activated charcoal; In benzene;
DOI:10.1016/S0040-4020(01)00600-7

Reference yield:

: 2627-86-3
(S)-1-phenyl-ethylamine

: 206127-71-1
isopropyl 7-[[(1'S)-1'-phenylethyl]amino]-6,7-dideoxy-1,2:3,4-di-O-isopropylidene-D-glycero-α-D-galactooctopyranuronate

Guidance literature:: Multi-step reaction with 2 steps

1: benzene / 13 h / Heating

2: H₂ / Pd/C / benzene / 8 h / 20 °C / 7500.6 Torr

With hydrogen; palladium on activated charcoal; In benzene;
DOI:10.1016/S0040-4020(01)00600-7