Tetraethylammonium benzoate

Base Information

• Chemical Name: Tetraethylammonium benzoate
• CAS No.: 16909-22-1
• Molecular Formula: C15H25NO2
• Molecular Weight: 251.369
• Hs Code.: 2923900090
• European Community (EC) Number: 240-957-3
• DSSTox Substance ID: DTXSID3066132
• Mol file: 16909-22-1.mol

Synonyms:Tetraethylammonium benzoate;16909-22-1;Ethanaminium, N,N,N-triethyl-, benzoate;Ethanaminium, N,N,N-triethyl-, benzoate (1:1);tetraethylazanium;benzoate;EINECS 240-957-3;tetraethylazanium benzoate;tetraethyl ammonium benzoate;SCHEMBL112480;TETRAETHYLAMMONIUMBENZOATE;C8H20N.C7H5O2;DTXSID3066132;AKOS028108528;C8-H20-N.C7-H5-O2;AS-80512;FT-0758231;E77568;J-010507;Tetraethylammonium benzoate, for electrochemical analysis, >=99.0%

Chemical Property of Tetraethylammonium benzoate

Chemical Property:

• Vapor Pressure: 0.01Pa at 20℃
• Boiling Point: °Cat760mmHg
• Flash Point: °C
• PSA: 40.13000
• Density: g/cm³
• LogP: 1.93290
• Solubility.: H2O: 0.1 g/mL, clear, colorless
• Water Solubility.: 963g/L at 20℃
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 4
• Exact Mass: 251.188529040
• Heavy Atom Count: 18
• Complexity: 145

Purity/Quality:

99.9% ^*data from raw suppliers

Tetraethylammonium benzoate for electrochemical analysis, ≥99.0% ^*data from reagent suppliers

Safty Information:

• Hazard Codes: Xi
• Statements: 36/37/38
• Safety Statements: 26-36

MSDS Files:

SDS file from LookChem

Total 1 MSDS from other Authors

Useful:

• Canonical SMILES: CC[N+](CC)(CC)CC.C1=CC=C(C=C1)C(=O)[O-]

Technology Process of Tetraethylammonium benzoate

There total 4 articles about Tetraethylammonium benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

tetraethylammonium hydroxide (77-98-5) + benzoic acid (65-85-0,8013-63-6) → benzoic acid tetraethylammonium salt (16909-22-1)

Guidance literature:

at 20 ℃; for 5h;

DOI:10.1016/S1872-2067(17)62822-5

Reference yield:

tetraethylammonium bromide (71-91-0) + silver benzoate (532-31-0) → benzoic acid tetraethylammonium salt (16909-22-1)

Guidance literature:

In water;

DOI:10.1134/S1070428021040047

Reference yield:

tetraethylammonium tosylate (733-44-8) + benzoic acid (65-85-0,8013-63-6) → benzoic acid tetraethylammonium salt (16909-22-1)

Guidance literature:

In N,N-dimethyl-formamide; Ambient temperature; electrolysis;

DOI:10.1246/cl.1985.371

upstream raw materials:

tetraethylammonium iodide

benzoic acid

tetraethylammonium tosylate

tetraethylammonium hydroxide

Downstream raw materials:

methyl (13S)-13-(benzoyloxy)-16-oxo-17-noratisan-18-oate

(Et₄N)[Mo(O₂CPh)(S₂C₂Me₂)2]

(Et₄N)[W(IV)(O₂CPh)(1,2-dimethyldithiolene)2]

(+/-)-(1RS,6RS,8RS,9RS)-Tricyclo<6.2.2.0^1,6>dodec-9-yl Benzoate

Refernces

• 1、 Sun, Wei,Xu, Fei,Cheng, Weiguo,Sun, Jian,Ning, Guoqing,Zhang, Suojiang. "Synthesis of isosorbide-based polycarbonates via melt polycondensation catalyzed by quaternary ammonium ionic liquids". . p. 908 - 917. Retrieved 2017/05/22.