N-(benzyl)benzyloxycarbonyl-5-aminopentyl 2-O-benzoyl-4-O-(2-O-benzoyl-4,6-di-O-benzyl-3-O-tert-butyldimethylsilyl-β-D-galactopyranosyl)-3-O-benzyl-β-D-xylopyranoside

Base Information

Chemical Name:N-(benzyl)benzyloxycarbonyl-5-aminopentyl 2-O-benzoyl-4-O-(2-O-benzoyl-4,6-di-O-benzyl-3-O-tert-butyldimethylsilyl-β-D-galactopyranosyl)-3-O-benzyl-β-D-xylopyranoside
CAS No.:1269467-08-4
Molecular Formula:C₇₂H₈₃NO₁₄Si
Molecular Weight:1214.53
Hs Code.:

N-(benzyl)benzyloxycarbonyl-5-aminopentyl 2-O-benzoyl-4-O-(2-O-benzoyl-4,6-di-O-benzyl-3-O-tert-butyldimethylsilyl-β-D-galactopyranosyl)-3-O-benzyl-β-D-xylopyranoside

Synonyms:N-(benzyl)benzyloxycarbonyl-5-aminopentyl 2-O-benzoyl-4-O-(2-O-benzoyl-4,6-di-O-benzyl-3-O-tert-butyldimethylsilyl-β-D-galactopyranosyl)-3-O-benzyl-β-D-xylopyranoside

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Chemical Property of N-(benzyl)benzyloxycarbonyl-5-aminopentyl 2-O-benzoyl-4-O-(2-O-benzoyl-4,6-di-O-benzyl-3-O-tert-butyldimethylsilyl-β-D-galactopyranosyl)-3-O-benzyl-β-D-xylopyranoside

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Technology Process of N-(benzyl)benzyloxycarbonyl-5-aminopentyl 2-O-benzoyl-4-O-(2-O-benzoyl-4,6-di-O-benzyl-3-O-tert-butyldimethylsilyl-β-D-galactopyranosyl)-3-O-benzyl-β-D-xylopyranoside

There total 14 articles about N-(benzyl)benzyloxycarbonyl-5-aminopentyl 2-O-benzoyl-4-O-(2-O-benzoyl-4,6-di-O-benzyl-3-O-tert-butyldimethylsilyl-β-D-galactopyranosyl)-3-O-benzyl-β-D-xylopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 920958-49-2
benzyl-(5-hydroxy-pentyl)-carbamic acid benzyl ester

: 1269466-99-0
p-methylphenyl 2-O-benzoyl-4-O-(2-O-benzoyl-4,6-di-O-benzyl-3-O-tert-butyldimethylsilyl-β-D-galactopyranosyl)-3-O-benzyl-1-thio-β-D-xylopyranoside

: 1269467-08-4
N-(benzyl)benzyloxycarbonyl-5-aminopentyl 2-O-benzoyl-4-O-(2-O-benzoyl-4,6-di-O-benzyl-3-O-tert-butyldimethylsilyl-β-D-galactopyranosyl)-3-O-benzyl-β-D-xylopyranoside

: 1308401-27-5
C₇₂H₈₃NO₁₄Si

Guidance literature:: benzyl-(5-hydroxy-pentyl)-carbamic acid benzyl ester; p-methylphenyl 2-O-benzoyl-4-O-(2-O-benzoyl-4,6-di-O-benzyl-3-O-tert-butyldimethylsilyl-β-D-galactopyranosyl)-3-O-benzyl-1-thio-β-D-xylopyranoside; With N-iodo-succinimide; In dichloromethane; acetonitrile; at -40 ℃; for 0.166667h; Inert atmosphere;

With trifluorormethanesulfonic acid; In dichloromethane; acetonitrile; at -40 ℃; for 3h; Inert atmosphere;
DOI:10.1021/ol200192d

Reference yield: 71.0%

: 1269466-90-1
p-methylphenyl 2-O-benzoyl-4,6-di-O-benzyl-3-O-tert-butyldimethylsilyl-1-thio-β-D-galactoside

: 1269467-05-1
N-(benzyl)benzyloxycarbonyl-5-aminopentyl 2-O-benzoyl-3-O-benzyl-β-D-xylopyranoside

: 1269467-08-4
N-(benzyl)benzyloxycarbonyl-5-aminopentyl 2-O-benzoyl-4-O-(2-O-benzoyl-4,6-di-O-benzyl-3-O-tert-butyldimethylsilyl-β-D-galactopyranosyl)-3-O-benzyl-β-D-xylopyranoside

Guidance literature:: p-methylphenyl 2-O-benzoyl-4,6-di-O-benzyl-3-O-tert-butyldimethylsilyl-1-thio-β-D-galactoside; N-(benzyl)benzyloxycarbonyl-5-aminopentyl 2-O-benzoyl-3-O-benzyl-β-D-xylopyranoside; With N-iodo-succinimide; In dichloromethane; at -78 ℃; for 0.166667h; Inert atmosphere;

With trifluorormethanesulfonic acid; In dichloromethane; at -78 - -20 ℃; for 2h; Inert atmosphere;
DOI:10.1021/ol200192d

Reference yield: 48.0%

: 920958-49-2
benzyl-(5-hydroxy-pentyl)-carbamic acid benzyl ester

: 1269466-61-6
4-methylphenyl 2-O-benzoyl-3-O-benzyl-1-thio-β-D-xylopyranoside

: 1269466-90-1
p-methylphenyl 2-O-benzoyl-4,6-di-O-benzyl-3-O-tert-butyldimethylsilyl-1-thio-β-D-galactoside

: 1269467-08-4
N-(benzyl)benzyloxycarbonyl-5-aminopentyl 2-O-benzoyl-4-O-(2-O-benzoyl-4,6-di-O-benzyl-3-O-tert-butyldimethylsilyl-β-D-galactopyranosyl)-3-O-benzyl-β-D-xylopyranoside

Guidance literature:: 4-methylphenyl 2-O-benzoyl-3-O-benzyl-1-thio-β-D-xylopyranoside; p-methylphenyl 2-O-benzoyl-4,6-di-O-benzyl-3-O-tert-butyldimethylsilyl-1-thio-β-D-galactoside; With N-iodo-succinimide; In dichloromethane; at -78 ℃; for 0.166667h; Inert atmosphere;

With trifluorormethanesulfonic acid; In dichloromethane; at -78 ℃; for 3h; Inert atmosphere;

benzyl-(5-hydroxy-pentyl)-carbamic acid benzyl ester; In dichloromethane; at -78 - -20 ℃;
DOI:10.1021/ol200192d