9,9-bis[[N-(2,6-diisopropylphenyl)-1,6-di(4-formylphenoxy)]perylene-3,4-dicarboximide]

Base Information

• Chemical Name: 9,9-bis[[N-(2,6-diisopropylphenyl)-1,6-di(4-formylphenoxy)]perylene-3,4-dicarboximide]
• CAS No.: 1398077-16-1
• Molecular Formula: C₉₆H₆₈N₂O₁₂
• Molecular Weight: 1441.6

Synonyms:9,9-bis[[N-(2,6-diisopropylphenyl)-1,6-di(4-formylphenoxy)]perylene-3,4-dicarboximide]

Chemical Property of 9,9-bis[[N-(2,6-diisopropylphenyl)-1,6-di(4-formylphenoxy)]perylene-3,4-dicarboximide]

Chemical Property:

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Technology Process of 9,9-bis[[N-(2,6-diisopropylphenyl)-1,6-di(4-formylphenoxy)]perylene-3,4-dicarboximide]

There total 3 articles about 9,9-bis[[N-(2,6-diisopropylphenyl)-1,6-di(4-formylphenoxy)]perylene-3,4-dicarboximide] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

N-(2,6-diisopropylphenyl)-1,6-bis(4-formylphenoxy)-9-bromoperylene-3,4-dicarboximide (1398077-13-8) + N-(2,6-diisopropylphenyl)-1,6-bis(4-formylphenoxy)-9-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)perylene-3,4-dicarboximide (1398077-14-9) → 9,9-bis[[N-(2,6-diisopropylphenyl)-1,6-di(4-formylphenoxy)]perylene-3,4-dicarboximide] (1398077-16-1)

Guidance literature:

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; In ethanol; water; toluene; at 80 ℃; for 24h; Inert atmosphere;

DOI:10.1039/c2cc34094a

Reference yield: 54.0%

N-(2,6-diisopropylphenyl)-1,6-bis(4-formylphenoxy)-9-bromoperylene-3,4-dicarboximide (1398077-13-8) + bis(pinacol)diborane (73183-34-3) → N-(2,6-diisopropylphenyl)-1,6-bis(4-formylphenoxy)-9-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)perylene-3,4-dicarboximide (1398077-14-9) + 9,9-bis[[N-(2,6-diisopropylphenyl)-1,6-di(4-formylphenoxy)]perylene-3,4-dicarboximide] (1398077-16-1)

Guidance literature:

With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate; In 1,4-dioxane; at 70 ℃; for 24h; Inert atmosphere;

DOI:10.1039/c2cc34094a

Reference yield: 14.0%

N-(2,6-diisopropylphenyl)-1,6-bis(4-formylphenoxy)-9-bromoperylene-3,4-dicarboximide (1398077-13-8) → 9,9-bis[[N-(2,6-diisopropylphenyl)-1,6-di(4-formylphenoxy)]perylene-3,4-dicarboximide] (1398077-16-1)

Guidance literature:

With [2,2]bipyridinyl; bis(1,5-cyclooctadiene)nickel ⁽⁰⁾; cyclo-octa-1,5-diene; In N,N-dimethyl-formamide; at 65 ℃; for 4h; Inert atmosphere;

DOI:10.1039/c2cc34094a

upstream raw materials:

N-(2,6-diisopropylphenyl)-1,6-bis(4-formylphenoxy)-9-bromoperylene-3,4-dicarboximide

bis(pinacol)diborane

N-(2,6-diisopropylphenyl)-1,6-bis(4-formylphenoxy)-9-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)perylene-3,4-dicarboximide

Downstream raw materials:

N,N’-(2,6-diisopropylphenyl)-1,6,11,16-tetra(4-formylphenoxy)quaterrylene

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