tert-butyl 4-[4'-(3''-hydroxy-4''-methyl-4''-phenylsulfanyl-pentanoylamino)-4'-methyl-pentanoylamino]-4-methyl-pentanoate

Base Information

Chemical Name:tert-butyl 4-[4'-(3''-hydroxy-4''-methyl-4''-phenylsulfanyl-pentanoylamino)-4'-methyl-pentanoylamino]-4-methyl-pentanoate
CAS No.:910865-33-7
Molecular Formula:C₂₈H₄₆N₂O₅S
Molecular Weight:522.75
Hs Code.:

Synonyms:tert-butyl 4-[4'-(3''-hydroxy-4''-methyl-4''-phenylsulfanyl-pentanoylamino)-4'-methyl-pentanoylamino]-4-methyl-pentanoate

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Chemical Property of tert-butyl 4-[4'-(3''-hydroxy-4''-methyl-4''-phenylsulfanyl-pentanoylamino)-4'-methyl-pentanoylamino]-4-methyl-pentanoate

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Technology Process of tert-butyl 4-[4'-(3''-hydroxy-4''-methyl-4''-phenylsulfanyl-pentanoylamino)-4'-methyl-pentanoylamino]-4-methyl-pentanoate

There total 11 articles about tert-butyl 4-[4'-(3''-hydroxy-4''-methyl-4''-phenylsulfanyl-pentanoylamino)-4'-methyl-pentanoylamino]-4-methyl-pentanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 627539-06-4
tert-butyl 4-methyl-4-nitropentanoate

: 910865-33-7
tert-butyl 4-[4'-(3''-hydroxy-4''-methyl-4''-phenylsulfanyl-pentanoylamino)-4'-methyl-pentanoylamino]-4-methyl-pentanoate

Guidance literature:: Multi-step reaction with 6 steps

1: 60 percent / H₂ / Raney nickiel / ethanol

2: 3.60 g / triethylamine / tetrahydrofuran / 20 °C

3: 69 percent / SOCl₂ / 48 h / 40 °C

4: 82 percent / KOH; H₂O / methanol / 20 °C

5: DCC / tetrahydrofuran / 20 °C

6: 1.40 g / triethylamine / tetrahydrofuran / 20 °C

With potassium hydroxide; thionyl chloride; water; hydrogen; triethylamine; dicyclohexyl-carbodiimide; Raney nickiel; In tetrahydrofuran; methanol; ethanol;
DOI:10.1039/b606882k

Reference yield:

: 1663-39-4,25232-27-3
tert-Butyl acrylate

: 910865-33-7
tert-butyl 4-[4'-(3''-hydroxy-4''-methyl-4''-phenylsulfanyl-pentanoylamino)-4'-methyl-pentanoylamino]-4-methyl-pentanoate

Guidance literature:: Multi-step reaction with 3 steps

1: 95 percent / DBU / CH₂Cl₂

2: 60 percent / H₂ / Raney nickiel / ethanol

3: 1.40 g / triethylamine / tetrahydrofuran / 20 °C

With hydrogen; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; Raney nickiel; In tetrahydrofuran; ethanol; dichloromethane;
DOI:10.1039/b606882k