C₂₄H₂₄IO₅P

Base Information

Chemical Name:C₂₄H₂₄IO₅P
CAS No.:1356412-05-9
Molecular Formula:C₂₄H₂₄IO₅P
Molecular Weight:550.33
Hs Code.:

C<sub>24</sub>H<sub>24</sub>IO<sub>5</sub>P

Synonyms:C₂₄H₂₄IO₅P

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Chemical Property of C₂₄H₂₄IO₅P

Chemical Property:

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Technology Process of C₂₄H₂₄IO₅P

There total 10 articles about C₂₄H₂₄IO₅P which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1356412-04-8
[2,3-dihydro-2,3-dimethoxy-2,3-dimethylbenzo[b][1,4]dioxin-7-yl]diphenylphosphineoxide

: 1356412-05-9
C₂₄H₂₄IO₅P

Guidance literature:: [2,3-dihydro-2,3-dimethoxy-2,3-dimethylbenzo[b][1,4]dioxin-7-yl]diphenylphosphineoxide; With lithium diisopropyl amide; In tetrahydrofuran; at -70 ℃; for 3.5h; Inert atmosphere;

With iodine; In tetrahydrofuran; at -70 - 20 ℃; Inert atmosphere;
DOI:10.1016/j.tetlet.2011.11.111

Reference yield:

: 1356411-94-3
(2R,3R)-2,3-dihydro-2,3-dimethoxy-2,3-dimethylbenzo[b][1,4]dioxin-6-amine

: 1356412-05-9
C₂₄H₂₄IO₅P

Guidance literature:: Multi-step reaction with 4 steps

1.1: acetic acid; sodium nitrite / water; acetonitrile / 0.5 h / 0 - 5 °C / Inert atmosphere

1.2: 1 h / 55 - 60 °C / Inert atmosphere

2.1: n-butyllithium / tetrahydrofuran; hexane / 2 h / -75 °C / Inert atmosphere

2.2: 3.75 h / -75 - 0 °C / Inert atmosphere

3.1: dihydrogen peroxide / methanol; water / 2.5 h / 15 - 20 °C

4.1: lithium diisopropyl amide / tetrahydrofuran / 3.5 h / -70 °C / Inert atmosphere

4.2: -70 - 20 °C / Inert atmosphere

With n-butyllithium; dihydrogen peroxide; acetic acid; lithium diisopropyl amide; sodium nitrite; In tetrahydrofuran; methanol; hexane; water; acetonitrile;
DOI:10.1016/j.tetlet.2011.11.111

Reference yield:

: 1394920-70-7
2-(2,3-dihydro-2,3-dimethoxy-2,3-dimethylbenzo[b][1,4]dioxin-7-ylcarbamoyl)benzoic acid

: 1356412-05-9
C₂₄H₂₄IO₅P

Guidance literature:: Multi-step reaction with 6 steps

1.1: isopropyl alcohol / 12 h / 20 °C / Inert atmosphere

2.1: sodium hydroxide / 18 h / 100 °C / Inert atmosphere

3.1: acetic acid; sodium nitrite / water; acetonitrile / 0.5 h / 0 - 5 °C / Inert atmosphere

3.2: 1 h / 55 - 60 °C / Inert atmosphere

4.1: n-butyllithium / tetrahydrofuran; hexane / 2 h / -75 °C / Inert atmosphere

4.2: 3.75 h / -75 - 0 °C / Inert atmosphere

5.1: dihydrogen peroxide / methanol; water / 2.5 h / 15 - 20 °C

6.1: lithium diisopropyl amide / tetrahydrofuran / 3.5 h / -70 °C / Inert atmosphere

6.2: -70 - 20 °C / Inert atmosphere

With n-butyllithium; dihydrogen peroxide; acetic acid; sodium hydroxide; lithium diisopropyl amide; sodium nitrite; In tetrahydrofuran; methanol; hexane; water; isopropyl alcohol; acetonitrile;
DOI:10.1016/j.tetlet.2011.11.111