Technology Process of C26H37ClN10O2
There total 4 articles about C26H37ClN10O2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C20H32N4O;
With
N-ethyl-N,N-diisopropylamine;
In
N,N-dimethyl-formamide;
at 20 ℃;
for 0.166667h;
3,5-diamino-6-chloro-N-[(methylsulfanyl)methanimidoyl]pyrazine-2-carboxamide;
In
N,N-dimethyl-formamide;
at 70 ℃;
for 3h;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: trifluorormethanesulfonic acid / 1 h / Cooling with ice
1.2: 4 h / 20 °C / Cooling with ice
2.1: sodium hydroxide; water / tert-butyl methyl ether; tetrahydrofuran / 20 °C
3.1: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 0.17 h / 20 °C
3.2: 3 h / 70 °C
With
trifluorormethanesulfonic acid; water; N-ethyl-N,N-diisopropylamine; sodium hydroxide;
In
tetrahydrofuran; tert-butyl methyl ether; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: sodium hydroxide; water / methanol / 3 h / Reflux
2.1: trifluorormethanesulfonic acid / 1 h / Cooling with ice
2.2: 4 h / 20 °C / Cooling with ice
3.1: sodium hydroxide; water / tert-butyl methyl ether; tetrahydrofuran / 20 °C
4.1: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 0.17 h / 20 °C
4.2: 3 h / 70 °C
With
trifluorormethanesulfonic acid; water; N-ethyl-N,N-diisopropylamine; sodium hydroxide;
In
tetrahydrofuran; methanol; tert-butyl methyl ether; N,N-dimethyl-formamide;