tert-butyl {2-[3-({[(2,6-dichlorobenzyl)amino]carbonyl}amino)-phenyl]ethyl}carbamate

Base Information

Chemical Name:tert-butyl {2-[3-({[(2,6-dichlorobenzyl)amino]carbonyl}amino)-phenyl]ethyl}carbamate
CAS No.:1185465-60-4
Molecular Formula:C₂₁H₂₅Cl₂N₃O₃
Molecular Weight:438.354
Hs Code.:

Synonyms:tert-butyl {2-[3-({[(2,6-dichlorobenzyl)amino]carbonyl}amino)-phenyl]ethyl}carbamate

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Chemical Property of tert-butyl {2-[3-({[(2,6-dichlorobenzyl)amino]carbonyl}amino)-phenyl]ethyl}carbamate

Chemical Property:

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Technology Process of tert-butyl {2-[3-({[(2,6-dichlorobenzyl)amino]carbonyl}amino)-phenyl]ethyl}carbamate

There total 6 articles about tert-butyl {2-[3-({[(2,6-dichlorobenzyl)amino]carbonyl}amino)-phenyl]ethyl}carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 6575-27-5
2,6-dichlorobenzylamine

: 1185465-25-1
tert-butyl [2-(3-isocyanatophenyl)ethyl]carbamate

: 1185465-60-4
tert-butyl {2-[3-({[(2,6-dichlorobenzyl)amino]carbonyl}amino)-phenyl]ethyl}carbamate

Guidance literature:: at 20 ℃;
DOI:10.1016/j.bmcl.2010.12.096

Reference yield:

: 180079-93-0
N-(3-nitrophenylmethyl)methylcarbamic acid t-butyl ester

: 1185465-60-4
tert-butyl {2-[3-({[(2,6-dichlorobenzyl)amino]carbonyl}amino)-phenyl]ethyl}carbamate

Guidance literature:: Multi-step reaction with 3 steps

1: palladium 10% on activated carbon; hydrogen / methanol / 3 h / 20 °C / 1551.49 Torr

2: triethylamine / dichloromethane / 2.5 h / 20 °C

3: 20 °C

With palladium 10% on activated carbon; hydrogen; triethylamine; In methanol; dichloromethane;
DOI:10.1016/j.bmcl.2010.12.096

Reference yield:

: 621-50-1
(3-nitrophenyl)acetonitrile

: 1185465-60-4
tert-butyl {2-[3-({[(2,6-dichlorobenzyl)amino]carbonyl}amino)-phenyl]ethyl}carbamate

Guidance literature:: Multi-step reaction with 5 steps

1: dimethylsulfide borane complex / tetrahydrofuran / 24 h / 20 °C

2: tetrahydrofuran / 2 h

3: palladium 10% on activated carbon; hydrogen / methanol / 3 h / 20 °C / 1551.49 Torr

4: triethylamine / dichloromethane / 2.5 h / 20 °C

5: 20 °C

With dimethylsulfide borane complex; palladium 10% on activated carbon; hydrogen; triethylamine; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1016/j.bmcl.2010.12.096