4-(2-bromoethoxy)benzaldehyde ethylene acetal

Base Information

Chemical Name:4-(2-bromoethoxy)benzaldehyde ethylene acetal
CAS No.:114258-53-6
Molecular Formula:C₁₁H₁₃BrO₃
Molecular Weight:273.126
Hs Code.:

Synonyms:4-(2-bromoethoxy)benzaldehyde ethylene acetal

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Chemical Property of 4-(2-bromoethoxy)benzaldehyde ethylene acetal

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Technology Process of 4-(2-bromoethoxy)benzaldehyde ethylene acetal

There total 2 articles about 4-(2-bromoethoxy)benzaldehyde ethylene acetal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 107-21-1
ethylene glycol

: 52191-15-8
4-(2-bromoethyloxy)benzaldehyde

: 114258-53-6
4-(2-bromoethoxy)benzaldehyde ethylene acetal

Guidance literature:: With phosphoric acid; In benzene; for 18h; Heating;
DOI:10.1248/cpb.35.2394

Reference yield:

: 123-08-0,65581-83-1
4-hydroxy-benzaldehyde

: 114258-53-6
4-(2-bromoethoxy)benzaldehyde ethylene acetal

Guidance literature:: Multi-step reaction with 2 steps

1: 21 percent / K₂CO₃ / dimethylformamide / 68 h / Ambient temperature

2: 90 percent / 85percent phosphoric acid / benzene / 18 h / Heating

With phosphoric acid; potassium carbonate; In N,N-dimethyl-formamide; benzene;
DOI:10.1248/cpb.35.2394