4-<3-methanesulfonamido>propyl>benzoic acid

Base Information

Chemical Name:4-<3-methanesulfonamido>propyl>benzoic acid
CAS No.:70108-05-3
Molecular Formula:C₂₀H₃₁NO₅S
Molecular Weight:397.536
Hs Code.:

4-<3-<N-<3-(1-hydroxycyclohexyl)propyl>methanesulfonamido>propyl>benzoic acid

Synonyms:4-<3-methanesulfonamido>propyl>benzoic acid

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-<3-methanesulfonamido>propyl>benzoic acid

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Technology Process of 4-<3-methanesulfonamido>propyl>benzoic acid

There total 5 articles about 4-<3-methanesulfonamido>propyl>benzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 70108-04-2
4-<3-methanesulfonamido>propyl>benzoic acid

: 70108-05-3
4-<3-methanesulfonamido>propyl>benzoic acid

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethyl acetate; at 27 ℃; for 0.0833333h; under 2275.5 Torr;
DOI:10.1021/jm00357a005

Reference yield:

: 6309-79-1
4-(3-Bromo-propyl)-benzoic acid

: 70108-05-3
4-<3-methanesulfonamido>propyl>benzoic acid

Guidance literature:: Multi-step reaction with 5 steps

1: 89 percent / conc. H₂SO₄ / benzene / 23 h / Heating

2: 1.) NaH / 1.) benzene, DMF, 90 deg C, 2.5 h, 2.) benzene, DMF, 90 deg C, 28 h

3: NaH / benzene; dimethylformamide / 1 h / 60 °C

4: NaOH / methanol; H₂O / 2 h / Heating

5: 2.9 g / H₂ / 5 percent Pd/C / ethyl acetate / 0.08 h / 27 °C / 2275.5 Torr

With sodium hydroxide; sulfuric acid; hydrogen; sodium hydride; palladium on activated charcoal; In methanol; water; ethyl acetate; N,N-dimethyl-formamide; benzene;
DOI:10.1021/jm00357a005

Reference yield:

: 56703-31-2
4-(3-Bromo-propyl)-benzoic acid ethyl ester

: 70108-05-3
4-<3-methanesulfonamido>propyl>benzoic acid

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) NaH / 1.) benzene, DMF, 90 deg C, 2.5 h, 2.) benzene, DMF, 90 deg C, 28 h

2: NaH / benzene; dimethylformamide / 1 h / 60 °C

3: NaOH / methanol; H₂O / 2 h / Heating

4: 2.9 g / H₂ / 5 percent Pd/C / ethyl acetate / 0.08 h / 27 °C / 2275.5 Torr

With sodium hydroxide; hydrogen; sodium hydride; palladium on activated charcoal; In methanol; water; ethyl acetate; N,N-dimethyl-formamide; benzene;
DOI:10.1021/jm00357a005