(S)-(-)-methyl 3-(N-tert-butyldimethylsiloxy-N-benzylamino)-3-phenylpropanoate

Base Information

Chemical Name:(S)-(-)-methyl 3-(N-tert-butyldimethylsiloxy-N-benzylamino)-3-phenylpropanoate
CAS No.:417725-79-2
Molecular Formula:C₂₃H₃₃NO₃Si
Molecular Weight:399.605
Hs Code.:

Synonyms:(S)-(-)-methyl 3-(N-tert-butyldimethylsiloxy-N-benzylamino)-3-phenylpropanoate

Suppliers and Price of (S)-(-)-methyl 3-(N-tert-butyldimethylsiloxy-N-benzylamino)-3-phenylpropanoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-(-)-methyl 3-(N-tert-butyldimethylsiloxy-N-benzylamino)-3-phenylpropanoate

Chemical Property:

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Technology Process of (S)-(-)-methyl 3-(N-tert-butyldimethylsiloxy-N-benzylamino)-3-phenylpropanoate

There total 1 articles about (S)-(-)-methyl 3-(N-tert-butyldimethylsiloxy-N-benzylamino)-3-phenylpropanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 77681-22-2,3376-26-9,85225-56-5
(Z)-N-benzylidenebenzylamine N-oxide

: 77086-38-5
ketene t-butyldimethylsilyl methyl acetal

: C₂₃H₃₃NO₃Si

: 417725-79-2
(S)-(-)-methyl 3-(N-tert-butyldimethylsiloxy-N-benzylamino)-3-phenylpropanoate

Guidance literature:: With Ti-(R)-BINOL-4-tert-butylcatechol; In toluene; at -78 ℃; for 24h; Title compound not separated from byproducts.;
DOI:10.1021/ja0176649

Reference yield:

: 417725-79-2
(S)-(-)-methyl 3-(N-tert-butyldimethylsiloxy-N-benzylamino)-3-phenylpropanoate

: 37088-66-7
(3S)-methyl 3-amino-3-phenylpropanoate

Guidance literature:: Multi-step reaction with 2 steps

1: Zn; H₂SO₄ / methanol / 2 h / 60 °C

2: hydrogen / Pd/C / methanol / 16 h / 20 °C

With sulfuric acid; hydrogen; zinc; palladium on activated charcoal; In methanol;
DOI:10.1021/ja0176649